热管型散热器换热性能的实验研究及数值模拟

本文对一种可用于LED组灯源的热管型散热器在大空间自然对流条件下的换热性能进行了实验研究和数值模拟,主要研究了散热器倾斜角度对其换热性能的影响.研究结果表明:散热器的倾斜角度对散热器的换热性能有较大影响,散热器换热性能随倾斜角度的增加先恶化再变好,在倾斜角度为30°左右时其换热性能最差;在相同倾斜角度下,辐射换热量随加热功率的增大呈近似线性增大,但辐射换热量占总换热量的比例较小,在7%以下.     

求解流动和传热问题的一种新的全隐算法-CLEAR(下)

本文上篇阐述了CLEAR算法的推导过程和计算步骤,本文下篇通过五个二维不可压缩流动和传热的算例,对CLEAR算法和SIMPLER算法进行了比较,比较的内容为,在相同的收敛条件下, CLEAR算法和SIMPLER算法收敛所需的迭代次数的比值和对应的CPU时间的比值,以及这两个比值和时步倍率的关系,从而进一步研究了CLEAR算法的健壮性。计算结果表明,CLEAR算法可以在很大程度上加速迭代收敛,就所比较的算例而言,其可以节省迭代次数31％-85％,节省CPU时间17％-78％,而且该算法的健壮性可以通过引入第二松弛因子而得以提高。     

微燃机稳压箱的计算分析

本文对自行设计的100 kW微型燃气轮机的稳压箱进行了数值模拟,并将结果与国外某75 kW微型燃气轮机的稳压箱的数值模拟结果进行了对比。然后对结果进行分析,从中发现,自行设计的微型燃气轮机的稳压箱与国外同功率级的稳压箱相比,总压恢复系数有所提高,流动损失较小,因此具有更优良的气动性能。计算表明,进口处流动方向变化较大,流动损失也较大,并且流动复杂,有漩涡产生,流场具有复杂的结构,必须在设计时引起足够的重视。     

几种治疗脑血管病中成药中金属元素含量检测及临床意义

火焰原子吸收分光光度法测定了大活络丹、脑塞通、通脉宁心冲剂和脉通 4种中成药物中 Ca、Mg、Cu、Cr和 Mn5种元素的含量。 4种药物中均含有丰富的微量元素 ,为探讨中药微量元素与治疗脑血管疾病的关系提供了有用的数据。     

CPU散热器换热特性的实验研究

本文对两种不同类型的CPU散热器,整体平直翅片与分段式的平直翅片,在不同加热功率、不同流速下的强迫风冷的传热性能进行了实验研究,得出换热系数主要和来流速度有关,而与加热功率关系不大的结论,并将二者的换热性能进行了对比。结果表明,翅片2的换热系数随流速的变化更强烈,在其他相同条件下,其换热系数甚至可以达到翅片1的两倍。     

制备型高速逆流色谱分离纯化香菇多糖

利用高速逆流色谱仪,研究了双水相系统对香菇多糖的分离.溶剂系统为w(PEG1000):w(K2HPO4):w(KH2PO4):w(H2O)=0.5:1.25:1.25:7.0,在转速为500 r/min,流速为1.5 mL/min的条件下,成功分离了香菇多糖粗品(700 mg),得到LenⅠ(95 mg)、LenⅡ(45 mg)两个组分.用Sephadex G-100凝胶色谱柱检测纯度,结果显示:LenⅡ为单一峰,凝胶渗透色谱法测定; LenⅡ分子量为293 kDa;经酸水解后液相色谱分析表明,其单糖组成为葡萄糖和甘露糖,摩尔比为2.7:1; 红外光谱显示其具有多糖类的特征吸收峰.     

花状Cu2O/Cu的水热合成及其光催化性能

以硝酸铜为前驱体, 不采用任何模板, 通过逐步水热法合成了花状Cu2O/Cu复合纳米材料. 用扫描电镜(SEM)、X射线衍射(XRD)和紫外-可见漫反射光谱(DRS)对样品进行表征. 结果表明, 花状纳米Cu2O/Cu材料是由长为300-500 nm, 宽为30-70 nm的带状花瓣构成, 在可见光区域有很强的吸收. 复合材料中Cu的含量可以通过反应时间进行调控. 对染料Procion Red MX-5B(PR)的可见光催化降解, Cu能明显提高Cu2O的光催化性能. 当Cu质量分数为27%-71%时, 复合材料Cu2O/Cu的催化活性明显高于单相Cu2O. 与立方体形貌的Cu2O/Cu复合材料相比, 花状纳米Cu2O/Cu复合材料对染料PR有更高的催化降解性能. 且该复合材料有较高的循环回收利用率.     

Copper nitrate/acetic acid as an efficient synergistic catalytic system for the chemoselective tetrahydropyranylation of alcohols and phenols

Abstract  Tetrahydropyranylation of alcohols and phenols was accomplished successfully using copper nitrate and acetic acid as a synergistic catalyst at room temperature under solvent-free condition. Compared with other synergistic catalytic systems, copper nitrate/acetic acid proved to be the most efficient. Both alcohols (primary, secondary, tertiary, benzylic, cyclic, allyl, cinnamyl, and furyl) and phenols reacted smoothly in high yields. Graphical abstract        

Preparation of insulin-loaded PLA/PLGA microcapsules by a novel membrane emulsification method and its release in vitro

Uniform-sized biodegradable PLA/PLGA microcapsules loading recombinant human insulin (rhI) were successfully prepared by combining a Shirasu Porous Glass (SPG) membrane emulsification technique and a double emulsion-evaporation method. An aqueous phase containing rhI was used as the inner water phase (w1), and PLA/PLGA and Arlacel 83 were dissolved in a mixture solvent of dichloromethane (DCM) and toluene, which was used as the oil phase (o). These two solutions were emulsified by a homogenizer to form a w1/o primary emulsion. The primary emulsion was permeated through the uniform pores of a SPG membrane into an outer water phase by the pressure of nitrogen gas to form the uniform w1/o/w2 droplets. The solid polymer microcapsules were obtained by simply evaporating solvent from droplets. Various factors of the preparation process influencing the drug encapsulation efficiency and the drug cumulative release were investigated systemically. The results indicated that the drug encapsulation efficiency and the cumulative release were affected by the PLA/PLGA ratio, NaCl concentration in outer water phase, the inner water phase volume, rhI-loading amount, pH-value in outer water phase and the size of microcapsules. By optimizing the preparation process, the drug encapsulation efficiency was high up to 91.82%. The unique advantage of preparing drug-loaded microcapsules by membrane emulsification technique is that the size of microcapsules can be controlled accurately, and thus the drug cumulative release profile can be adjusted just by changing the size of microcapsules. Moreover, much higher encapsulation efficiency can be obtained when compared with the conventional mechanical stirring method.     

Phase regulated suppression and enhancement switches of four-wave mixing and fluorescence

We experimentally study the phase regulated switch between elcctromagnctically induced trans- parency and electromagmetically induced absorption in probe transmission signal and the conver- sion between enhancement and suppression in four-wave mixing and fluorescence signals for the first time. By changing the relative phase, electromagnetically induced transparency can be eonverted into electromagnetically induced absorption. In this process, the conversion from suppression to enhancement is also obtained in four-wave mixing and fluorescence signals. This research can be applied in non-linear optical device like optical switch and optical wavelength convertor.