Synthesen des 4-Sulfanilamido-5,6-dimethoxypyrimidins

Zusammenfassung Es wird über 4 verschiedene Synthesen des 4-Sulfanilamido-5,6-dimethoxypyrimidins² berichtet.Frau Prof. Dr. Dr.E. Cremer zum Geburtstage in Verehrung gewidmet.14. Mitt.:H. Bretschneider, J. Dehler undW. Klötzer, Mh. Chem.95, 207 (1964).     

Separated two-phase flow model: application to critical two-phase flow

A separated flow model has been developed to allow the calculation of critical flow rates for steam-water mixtures. This model considers hydrodynamic as well as thermal non-equilibrium effects which are present due to rapid depressurization. Thus, this model incorporates interphase interaction terms for momentum, energy and mass. The mass transfer, evaporation or condensation rate, is coupled with the heat transfer between the two phases. Certain empiricisms are necessary to be included into this model, e.g. the size and number of nucleation sites at the onset of flashing. Transitions from one flow regime to the other are assumed to occur at certain void fractions. Justification of these assumptions is only possible by comparison with experimental results of different authors which in general shows good agreement.     

First observation of 54Zn and its decay by two-proton emission

The nucleus 54Zn has been observed for the first time in an experiment at the SISSI/LISE3 facility of GANIL in the quasifragmentation of a 58Ni beam at 74.5 MeV/nucleon in a (nat)Ni target. The fragments were analyzed by means of the ALPHA-LISE3 separator and implanted in a silicon-strip detector where correlations in space and time between implantation and subsequent decay events allowed us to generate almost background free decay spectra for about 25 different nuclei at the same time. Eight 54Zn implantation events were observed. From the correlated decay events, the half-life of 54Zn is determined to be 3.2(+1.8)(-0.8) ms. Seven of the eight implantations are followed by two-proton emission with a decay energy of 1.48(2) MeV. The decay energy and the partial half-life are compared to model predictions and allow for a test of these two-proton decay models.     

"Safe" Coulomb excitation of 30Mg

We report on the first radioactive beam experiment performed at the recently commissioned REX-ISOLDE facility at CERN in conjunction with the highly efficient gamma spectrometer MINIBALL. Using 30Mg ions accelerated to an energy of 2.25 MeV/u together with a thin (nat)Ni target, Coulomb excitation of the first excited 2+ states of the projectile and target nuclei well below the Coulomb barrier was observed. From the measured relative deexcitation gamma-ray yields the B(E2;0(+)gs-->2(+)1) value of 30Mg was determined to be 241(31)e2 fm4. Our result is lower than values obtained at projectile fragmentation facilities using the intermediate-energy Coulomb excitation method, and confirms the theoretical conjecture that the neutron-rich magnesium isotope 30Mg resides outside the "island of inversion."     

In situ characterization of semiconductor saturable absorber mirrors in an operating Yb:KGW mode-locked laser

We report in situ characterization of a semiconductor saturable absorber mirror (SESAM) in an operating Yb:KGW mode-locked laser. The technique may be described as a pump-probe experiment in which the intracavity beam acts as a pump beam while the output of the same laser is used as a test beam for the SESAM reflectivity. At zero delay, the probe pulse overlaps in time with the subsequent intracavity pulse. The method is an alternative to standard pump-probe measurements in situations where the intracavity parameters such as energy fluence onto the SESAM, pulse length, and center wavelength cannot be achieved simultaneously with available lasers.     

Fine structure in the energy region of the isoscalar giant quadrupole resonance: characteristic scales from a wavelet analysis

Fine structure in the energy region of the isoscalar giant quadrupole resonance in nuclei is observed in high-resolution proton scattering experiments at iThemba LABS over a wide mass range. A novel method based on wavelet transforms is introduced for the extraction of scales characterizing the fine structure. A comparison with microscopic model calculations including two-particle two-hole (2p2h) degrees of freedom identifies the coupling to surface vibrations as the main source of the observed scales. A generic pattern is also found for the stochastic coupling to the background of the more complex states.     

Measurement of RLT and ATL in the 4He(e, e’p)3H reaction at pmiss of 130-300 MeV/ c

We have measured the ⁴He(e, ep)³H reaction at missing momenta of 130-300 MeV/c using the three-spectrometer facility at the Mainz microtron MAMI. Data were taken in perpendicular kinematics to allow us to determine the response function R_LT and the asymmetry term A_TL. The data are compared to both relativistic and non-relativistic calculations.     

The anisotropic quantum antiferromagnet on the Sierpiński gasket: Ground state and thermodynamics

We investigate an antiferromagnetic s = 1/2 quantum spin system with anisotropic spin exchange on a fractal lattice, the Sierpiski gasket. We introduce a novel approximative numerical method, the configuration selective diagonalization (CSD) and apply this method to a the Sierpiski gasket with N = 42. Using this and other methods we calculate ground state energies, spin gap, spin-spin correlations and specific heat data and conclude that the s = 1/2 quantum antiferromagnet on the Sierpinski gasket shows a disordered magnetic ground state with on the Sierpinski gasket shows a disordered magnetic ground state with a very short correlation length of and an, albeit very small, spin gap. This conclusion holds for Heisenberg as well a for XY exchange.Received: 18 February 2004, Published online: 20 April 2004PACS: 75.10.-b General theory and models of magnetic ordering - 05.45.Df Fractals - 75.40.Mg Numerical simulation studies