电感耦合等离子体发射光谱法同时测定涂料中的Pb、Cd、Cr和Hg

研究了电感耦合等离子体发射光谱法测定涂料中的重金属Pb，Cd，Cr和Hg，确定了测定涂料中的重金属Pb，Cd，Cr和Hg的最佳条件。加标回收试验和实际样品测定结果表明，方法的回收率和精密度分别在99.5％-110．0％和0．95％-1．98％范围，该方法快速、准确、可靠，各元素的检出限能满足涂料安全标准，适用于涂料的日常检验。     

将SVRT模型应用到单原子多原子反应F+CH2D2→CH2D/CHD2+DF/HF中

由于含时波包方法具有经典的直观又不乏量子力学的准确 ,选择含时波包方法来处理F +CH2 D2 →CH2 D/CHD2 +DF/HF反应 .把半刚性振转子 (SVRT)模型应用到该反应体系中 ,研究了两个通道中该反应从基态反应物开始在修正过的J1(MJ1)势能面上计算出来了反应几率、积分截面、速率常数 .反应几率随能量变化的图的数值结果给出了振荡结构 ,这些振荡结构是可以和动力学振荡联系起来的 .而这些振荡结构在积分截面随着能量变化的图中就被反应几率求和后的平均结果所掩盖了 .速率常数和实验结果的比较也得到了较好的结果 .     

无失效数据的Bayes和多层Bayes分析

本文推广了文献[6]的结果，对指数分布无失效数据的失效率，给出了Bayes估计、Bayes置信上限以及多层Bayes估计，从而可以得到无失效数据可靠度的估计，最后，结合实际问题进行了计算。     

自体静脉移植血管的拉伸实验研究

本文考察了自体移植静脉的纵向应力应变关系。将狗股静脉移植于股动脉，在术后不同时间切取移植静脉进行纵向单轴拉伸实验。结果表明，移植静脉的应力－应变曲线比正常静脉靠近应力坐标轴并在术后逐渐向左移动。这显示了移植血管管壁组织在术后的逐渐硬化。     

离焦散斑技术研究Kirchhoff板在动载作用期的弯曲

本文使用动态离焦散斑技术,测试板的动态弯曲获得成功。并推导了Kirchhoff板动态变形的有关分析,提出了由最大斜率确定材料常数的思想。显然,这是同离焦散斑方法所测数据直接相关的处理手法。     

Isolation and Structure Elucidation of Nortriterpenoids from Schisandra rubriflora

Seven new highly oxygenated nortriterpenoids, rubriflorins D–J ( 1 – 7 ), were isolated from the leaves and stems of Schisandra rubriflora, and their structures were elucidated on the basis of extensive analysis of spectroscopic data. These new compounds feature the opening of ring A compared with related known nortriterpenoids isolated from the genus Schisandra and showed weak activity against HIV‐1.     

Theoretical and Experimental Driving-Point Impedance Results of Resonance Circuits in a Gunn Waveguide Oscillator

The frequency tuning range of waveguide oscillator and its stability depend sensitively on the dimension of the resonance cap. Therefore the driving-point impedances with the various dimensions of the resonance cap are calculated by using HFSS(High Frequency Simulation System). In this paper the comparisons between theoretical results of the driving-point impedances as a function of frequency and that of experimental results are described. The oscillation frequency range could be predicted by using the theoretical evaluation methods which are proposed. It shows that resonance cap size and disc height have an effect on the frequency tuning characteristics of Gunn oscillator.     

X-ray absorption spectra of plasmas

In this paper we present a theoretical method to calculate the absorption spectra of hot dense plasmas. Based on our fully relativistic treatment incorporated with the quantum defect theory to handle the huge number of transition arrays from many configurations with high principal quantum number, we can calculate the absorption spectra for any element or multi-element plasmas with little computational efforts. We calculate the absorption spectra of C10H1605 plasmas, which are in good agreement with the experimental spectra. We can then provide diagnostic analysis for plasmas in relevant inertial confinement fusion (lCF) experiments; namely not only to determine plasmas' temperatures and densities, but also to provide the population densities of various ionic stages. Our theoretical method verified by "benchmark experiments" will be a basic tool to provide "precise" opacity data for the ICF research.``     

Synthesis of the D-Galactopyranoside Derivative of C_(60)

ThefascinatingsbocturesandpropertiesoffullereneshaveoPeneduPanewfieldofchendstry.Inparticular,F.Wudletal.l'2haveshownthatwatersofubleC6ocomPoundsinhibittheHITVen-zymesprotease(HIVP)andreversetranscriPtase(HIVRT).IthasbeenafocusofstUdytoinvestigatethebiologicalactivitiesofthesenovelsubstances.Fortheirpossiblemedicaluses,tolinkC6omoleculetonaturalProductssuchassugars,pephdes,amioacides,andsoonisanimPortantmethodinthisfield.Vasella3reportedthefirstglucosidederivativeofC6o'InthispaPer,w…