高速双边缘光纤光栅波长解调技术

提出一种双边缘结构对光纤光栅传感进行波长解调的方案,利用被测光谱通过不同光谱特性的滤波器时输出不同光强的比值确定被测光的波长.该系统在解调时不存在任何机械移动部分,比扫描式的解调方法测量速度更快,运行时更稳定、更精确.     

A simplified method to calculate the field distribution of pistonlike source

I.IntroductionThesoundfieldproducedbyanidealbaflledplanartransducerhasbeenoneofthemostfundamentalproblernsinacousticsforaverylongtime.TheproblemcanbereducedtothewellknownRayleighintegralorKing'sintegral.Inmostcases,however,theirsolutionsarenotanalyticalandcdnnotberepreselltedinclosedformbygeneralorspecialfunctions.AsanexaInPleoftheuniformpistonsource)todescribethesoundbeamdistributionsinthenearandtransitionzones,itisnecessarytomakecalculationsbyusingthenumericalintegrations(point-by-poillt)o…     

Semidirect products and wreath products of strongly π-inverse monoids

In this paper we determine the necessary and sufficient conditions for the semidirect products and the wreath products of two monoids to be strongly -inverse. Furthermore, we determine the least group congruence on a strongly -inverse monoid, and we give some important isomorphism theorems.     

Molybdosphoric Acid Mixed with Titania Used as a Catalyst to Synthesize Diphenyl Carbonate via Transesterification of Dimethyl Carbonate and Phenol

The 12-molybdosphoric acid mixed with titania (MPA-TiO2) was found to be a novel and efficient catalyst for the synthesis of diphenyl carbonate (DPC) via transesterification of dimethyl carbonate (DMC) and phenol. The X-ray diffraction (XRD) and infrared (IR) techniques were employed to characterize the prepared catalysts. The effect of the weight ratio of the 12-molybdosphoric acid to titania on the transesterification was investigated. A 13.1% yield of DPC and an 11.6% yield of methyl phenyl carbonate (MPC) were obtained over MPA-TiO2 with the weight ratio of MPA to TiO2 as 5:1.     

费托(FT)合成及相关反应的研究进展(英文)

按催化剂分类介绍了改性ＦＴ合成及与其相关反应的近期研究成果。即通过调制催化剂组成和反应条件,由合成气直接合成其他有价值的化工原料如醇、烯烃、芳香烃和石蜡等。分子筛,如ＡＩ－ＭＣＭ－４１和ＺＳＭ－５／磷铝分子筛等在ＦＴ及其相关反应中扮演着越来越重要的角色,但由于金属作为反应活性中心,所以金属催化剂如Ｆｅ,Ｃｏ、Ｐｄ、Ｒｈ和Ｎｉ,双金属如Ｆｅ－Ｉｒ和Ｐｔ－Ｍｏ仍然是人们研究的重点。另外,一些新的反应方法和新的材料也被采用,如超临界方法及超微粒催化剂等。     

Quantum Fisher Information in the Symmetric Pure Three-Qubit State

We investigate the quantum Fisher information in the symmetric pure three-qubit state. It is shown that the quantum Fisher information and the mean spin direction are determined by the probability amplitudes and the relative phase of the symmetric pure three-qubit state; while the length of mean spin is only determined by the probability amplitudes.     

分光光度法测定人工晶状体中清洗剂磺基琥珀酸二辛酯钠残留

建立分光光度法分析眼科植入物人工晶体中清洗剂磺基琥珀酸二辛酯钠残留的方法。磺基琥珀酸二辛酯在酸性水溶液介质中与亚甲基蓝形成离子对,用三氯甲烷提取并在651 nm波长处测定其吸光度。磺基琥珀酸二辛酯钠的质量浓度在1.0~5.0μg/m L内与吸光度呈良好的线性关系,线性相关系数r~2=0.990 1,检出限为0.4μg/m L。测定结果的相对标准偏差为1.21%(n=6),日间重复性为2.06%(n=6);加标回收率为90%~97%。该方法检出限低,再现性好,适用于人工晶状体中磺基琥珀酸二辛酯钠残留量的测定。     

A sensitive and specific HPGPC‐FD method for the study of pharmacokinetics and tissue distribution of Radix Ophiopogonis polysaccharide in rats

Interest in antimyocardial ischemic activity of a graminan‐type fructan with a weight average molecular weight of 4.8 kDa extracted from Radix Ophiopogonis (ROP) has necessitated the study of its pharmacokinetics and tissue distribution. For that, a simple HPGPC–FD method was developed for the sensitive and specific determination of FITC‐ROP (fluorescein–isothiocyanate‐labeled ROP) in plasma and rat tissues (heart, liver, spleen, lung, kidney, brain and stomach). The analyte was separated on a Shodex Sugar KS‐802 high‐performance gel column with 0.1 M phosphate buffer (pH 7.0) as mobile phase at a flow rate of 0.5 mL/min, and fluorescence detection at λ_ex 495 nm and λ_em 515 nm. The calibration curve for FITC‐ROP was linear over the range 0.25–20.0 or 50.0 μg/mL in all studied biosamples with correlation coefficients >0.995. The inter‐day and intra‐day precisions of analysis were not more than 10%, and assay accuracy ranged from 93 to 105% for plasma and from 89 to 108% for tissue homogenates. This method has been confirmed here to be suitable for the study of pharmacokinetics and tissue distribution of ROP and the achieved results are highly instructive for the further pharmaceutical development of ROP, suggesting the promising application of the method to the increasingly important carbohydrate‐based drugs. Copyright © 2009 John Wiley & Sons, Ltd.     

A variational phase field method for curve smoothing

A variational phase field model is proposed for curve smoothing, in which a weight function is associated with the similarity measure term in the model so that important geometric features could be well preserved. Finite element approximation of the proposed model is given for its numerical implementation. Since the model has a linear weak variational form, the discretized system could be solved efficiently by many existing solution techniques. An effective algorithm is also developed, for the purpose of feature preservation, to automatically determine the weight from the given data. Various numerical examples are presented to demonstrate effectiveness and robustness of the proposed method.     

Preparation and characterization of a novel luminescent nanoparticles

In this paper, a new kind of fluorescent nanomaterial with morin modified alumina core and silica shell was prepared. Samples were characterized by transmission electron microscope (TEM), X-ray diffraction (XRD), Fourier transform infrared spectra (FT-IR), photoluminescent (PL) spectroscopy and fluorescence microscope. TEM results indicated that this material could be synthesized in nanometer range. PL spectra suggested that this new synthesized material was photostable and it showed nearly no dye leakage. This was because the dye molecules could form stable complex with the reactive aluminum cations on the surfaces of the alumina particles. The excitation and emission maxima of this new luminescent material were located at 420 and 493 nm, respectively. This new kind of luminescent nanomaterial was prepared by morin, AlCl₃ and tetraethyl orthosilicate, which was very important for the large-scale and economic preparation luminescent nanoparticles because these precursors were inexpensive and the preparation process was convenient.