无孔单分散亲水性中强阳离子交换树脂的制备及其在蛋白质快速分离中的应用研究

以3.0μm无孔单分散亲水性交联聚甲基丙烯酸环氧丙酯树脂为基质,将其表面经新的化学方法改性后制备了一种新型的无孔中强阳离子交换色谱填料。详细考察了该无孔填料对标准蛋白分离性能,有机溶剂、pH、流动相盐种类和流速等对蛋白质保留的影响。实验结果表明,在流速为4 mL/min时,线性梯度时间在2.0 min内可快速分离4种标准蛋白,蛋白质的保留符合阳离子交换色谱规律。将其应用于快速纯化鸡蛋清中的溶菌酶,取得较好效果。     

具有Rao简单结构的多元t-模型的参数区间估计

在统计推断中,模型中未知参数的区间估计是一个重要的研究内容.本文通过构造枢轴量研究了具有Rao简单结构多元￡-模型的参数区间估计,利用条件分布技巧,得到枢轴量的分布,从而获得模型中单个未知参数的置信区域以及参数的联合置信区域.     

关于H-矩阵的实用判定的注记

本文指出《H-矩阵的实用判定》一文的主要结果中的许多条件是多余的,我们用比较简捷的方法改进了该文的结果,并给出了一些新的H-矩阵的判定方法．     

基于核磁共振弹性成像技术的肝纤维化分级体模研究

肝纤维化程度以及纤维化速率的精确判断对于相应治疗手术的选择以及治疗预后评估都是至关重要的.临床上需要发展一种非侵入性的肝纤维化定量检查手段.核磁共振弹性成像技术成为实现肝纤维化分级研究的最具发展前景的技术之一.我们研制开发了可用于进行肝纤维化分级研究的实验平台,并讨论了激励装置和位移相位成像序列的技术细节,最后给出了体模的初步实验结果并对结果进行了分析.为后续体模深入研究和临床应用实验奠定基础.     

围长至少为5的平面图的injective-染色

图G的injective k-染色是指映射c:V(G)→{1,2,…,k},使有公共邻点的两个顶点u,v满足c(u)≠c(v),用X_i(G)表示使G有一个injective k-染色的最小正整数k.对g(G)≥5的平面图G,若△(G)≥20,证明了X_i(G)≤△+3.     

Some Results on Planar Graphs of Class 1

We consider only simple graphs in this paper unless otherwise stated,A plane gragh is a,particular drawing of a planar graph in the Euclidean plane. For a plane graph G, we denote its vertex set, edge set, face set, and maximum degree by V(G), E(G), F(G), and △(G) (or simply     

INTERNAL FRICTION AND ULTRASONIC ATTENUATION RELATED TO CARRIERS IN HIGH Tc SUPERCONDUCTORS

For both BiSrCaCuO and TlBaCaCuO samples, internal frictions (Q^-1) in the kHz range reveal a plateau (Q^-1_p) above T_c and a rapid drop below T_c with the turning points located just at T_c for various samples with different T_c. This anomaly cannot be observed in non-superconducting samples. The ultrasonic attenuation (α) in TlBaCaCuO displays similar results to the internal friction. Moreover, it is discovered that the Q^-1_p is nearly proportional to the carrier density for Y(Pr)BaCuO and Gd(Pr)BaCuO with different Pr contents. These results show that the drop of Q^-1 and a below T_c is closely related to superconducting condensation. The Q^-1_p and α_p can be explained using coupling-model of carriers with local dynamic distortion because high T_c superconductors are strong-correlation systems. Furthermore, by taking account of the smearing of superconducting gap structure resulting from the recombination of quasi-particles and by modifying the BCS relative jump rate as S(E, E', Γ) = Re{1-Δ²/[(E-iΓ)(E'-iΓ)]}, the calculated results of internal friction and ultrasonic attenuation below T_c are in good agreement with the experimental data. The superconducting gap Δ and the damping rate Γ for both BiSrCaCuO and TlBaCaCuO have also been obtained, they are in accordance with those got by tunneling spectrum and NMR methods, etc.     

物理学上的重大实验

 物理学离不开实验。在物理学发展过程中，产生了许多重大实验。了解并重温这些著名实验，也许对     

以身许国

 1961年初春,“已是悬崖百丈冰”,天气窄冷.苏联杜布纳联合核子研究所中国专家组组长王淦昌回到阔别已久的北京,开始准备建造加速器的工作.