Time-dependent ratchetting experiments of SS304 stainless steel

The time-dependent strain cyclic characteristics and ratchetting behaviours of SS304 stainless steel were investigated by uniaxial/multiaxial cyclic loading tests at room and elevated temperatures (350 and 700 °C). The effects of loading rate, peak/valley strain or stress holds, ambient temperature and non-proportional loading path on the cyclic softening/hardening and ratchetting behaviours of the material were discussed. It is shown that: the cyclic deformation of the material presents remarkable time-dependence at room temperature and 700 °C; the cyclic hardening feature and ratchetting strain depend significantly on straining or stressing rate, hold-time, ambient temperature and the non-proportionality of loading path; the time-dependent ratchetting is resulted from the slight opening of hysteresis loop and visco-plasticity together, and the viscosity is a dominating factor at 700 °C; at 350 °C, abnormal rate-dependence and quick shakedown of ratchetting are observed due to the dynamic strain aging of the material at this temperature. Some significant conclusions are obtained, which are useful to construct a constitutive model to describe the time-dependent ratchetting behaviour of the material. It is also stated that the unified visco-plastic constitutive model discussed here cannot provide reasonable simulation to the time-dependent ratchetting at 700 °C, especially to that with certain peak/valley stress hold, since the effect of the high viscosity on time-dependent ratchetting cannot be properly described by using a unified visco-plastic flow rule.     

Strain-rate history and temperature effects on the torsional-shear behavior of a mild steel

Previous investigations on the effects of strain-rate and temperature histories on the mechanical behavior of steel are briefly reviewed. A study is presented on the influence of strain rate and strain-rate history on the shear behavior of a mild steel, over a wide range of temperature Experiments were performed on thin-walled tubular specimens of short gage length, using a torsional split-Hopkinson-bar apparatus adapted to permit quasi-static as well as dynamic straining at different temperatures. The constant-rate behavior was first measured at nominal strain rates of 10^?3 and 10³ s^?1 for ?150, ?100, ?50, 20, 200 and 400°C. Tests were then carried out, at the same temperatures, in which the strain rate was suddenly increased during deformation from the lower to the higher rate at various large values of plastic strain. The increase in rate occurred in a time of the order of 20 μs so that relatively little change of strain took place during the jump. The low strain-rate results show a well-defined elastic limit but no yield drop, a small yield plateau is found at room temperature. The subsequent strain hardening shows a maximum at 200°C, when serrated flow occurs and the ductility is reduced. The high strain-rate results show a considerable drop of stress at yield. The post-yield flow stress decreases steadily with increasing temperature, throughout the temperature range investigated. At room temperature and below, the strain-hardening rate becomes negative at large strains. The adiabatic temperature rise in the dynamic tests was computed on the assumption that the plastic work is entirely converted to heat. This enabled the isothermal dynamic stress-strain curves to be calculated, and showed that considerable thermal softening took place. The initial response to a strain-rate jump is approximately elastic, and has a magnitude which increases with decrease of testing temperature; it is little affected by the amount of prestrain. At 200 and 400° C, a yield drop occurs after the initial stress increment. The post-jump flow stress is always greater than that for the same strain in a constant-rate dynamic test, the strain-hardening rate becoming negative at large strains or low testing temperature. This observed effect of strain-rate history cannot be explained by the thermal softening accompanying dynamic deformation. These and other results concerning total ductility under various strain-rate and temperature conditions show that strain-rate history strongly affects the mechanical behavior of the mild steel tested and, hence, should be taken into account in the formulation of constitutive equations for that material.     

Notch strengthening in titanium aluminides under monotonic loading

An important concern for titanium aluminides is their limited ductility and its consequences for TiAl components containing stress concentrators. In recent experiments, evidence of notch strengthening has been found in one TiAl alloy under monotonic loading. The goal of this study is to fully explore this issue through tests on two cast alloys, one with a microstructure consisting of predominantly equiaxed gamma grains and the other having a fully lamellar microstructure. Tests involve monotonic tensile loading of notched specimens at room temperature under conditions of plane stress, where the notch radii are large relative to grain size. For each material, results from the testing of three notched specimen geometries are presented and finite element models are used to interpret the test results. This includes using the numerical models to apply Weibull statistical methods to predict notch strengthening in the specimens. It is shown that notch strengthening is clearly seen in both alloys tested and thus is likely to be a characteristic of TiAl alloys in general; however, strengthening is not as great as would be predicted by Weibull statistical methods as applied to brittle materials.     

Thermo-mechanical response of nylon 101 under uniaxial and multi-axial loadings: Part I,Experimental results over wide ranges of temperatures and strain rates

A comprehensive study of the thermo-mechanical response of a thermoplastic polymer, nylon 101 is presented. Quasi-static and dynamic compression uniaxial and multi-axial experiments (stress states) were performed at a wide range of strain rates (10⁻⁵ to 5000 s⁻¹) and temperatures (−60 to 177 °C or −76 to 350 °F). The material is found to be non-linearly dependent on strain rate and temperature. The change in volume after plastic deformation is investigated and is found to be negligibly small. The relaxation and creep responses at room temperature are found to be dependent on strain rate and the stress–strain level at which these phenomena are initiated. Total deformation is decomposed into visco-elastic and visco-plastic components; these components have been determined at different levels of deformation. Results from non-proportional uniaxial to biaxial compression, and torsion experiments, are also reported for three different strain rates at room temperature. It is shown that nylon 101 has a response dependent on the hydrostatic pressure.     

High strain-rate behavior of ice under uniaxial compression

In the present study, a modified split Hopkinson pressure bar (SHPB) is employed to investigate the dynamic response of ice under uniaxial compression in the range of strain rates from 60 to 1400 s^?1 and at initial test temperatures of ?10 and ?30 °C. The compressive strength of ice shows positive strain-rate sensitivity over the range of strain rates employed; a slight influence of ice microstructure is observed, but it is much less than that reported previously for ice deformation under quasi-static loading conditions [Schulson, E.M., IIiescu, D., Frott, A., 2005. Characterization of ice for return-to-flight of the space shuttle. Part 1 – Hard ice. NASA CR-2005-213643-Part 1]. Specimen thickness, within the range studied, was found to have little or no effect on the peak (failure) strength of ice, while lowering the test temperature from ?10 to ?30 °C had a considerable effect, with ice behaving stronger at the lower test temperature. Moreover, unlike in the case of uniaxial quasi-static compression of ice, the effect of specimen end-constraint during the high rate compression was found to be negligible. One important result of these experiments, which may have important implications in modeling ice impacts, involves the post “peak-stress” behavior of the ice in that the ice samples do not catastrophically lose their load carrying capacity even after the attainment of peak stress during dynamic compression. This residual (tail) strength of the damaged/fragmented ice is sizable, and in some cases is larger than the quasi-static compression strength reported for ice. Moreover, this residual strength is observed to be dependent on sample thickness and the strain rate, being higher for thinner samples and at higher strain-rates during dynamic compression.     

Cyclic thermo-viscoplasticity of high density polyethylene

Observations are reported in uniaxial cyclic tensile tests (loading–unloading with various maximum strains) on high density polyethylene at temperatures ranging from room temperature up to 90 °C. It is demonstrated that the maximum stress per cycle and an apparent residual strain (measured at the instant when the tensile force vanishes under retraction) strongly decrease with temperature. The latter seems unexpected as the interval of temperatures covers the α-relaxation temperature, which is conventionally associated with activation of additional mechanisms for inelastic flow. A model is developed that captures the decrease in residual strain with temperature. Adjustable parameters in the stress–strain relations are found by fitting the experimental data. The effects of temperature and maximum strain per cycle on residual strains are studied numerically.     

Artificial aging and shear deformation behaviour of 6022 aluminium alloy

In this study, the artificial aging behaviour of 6022-T4 alloy is investigated over a wide temperature range. Hardness readings, TEM and XRD analyses were performed. It was shown that 6022-T4 alloy can be substantially hardened through a short aging treatment at temperatures in excess of 200 °C. The strain hardening curves of the 6022 alloy in different aging conditions were measured using the simple shear test and analysed in terms of their respective microstructures. The under-aged and pre-peak-aged exhibited a good combination of strength and strain hardening while the peak-aged alloy was characterised by maximum strength, albeit with a drastic reduction in strain hardening ability. Strain reversal experiments in simple shear were carried out in order to characterize the Bauschinger effect for the different heat treatment conditions. It was shown that the T4 and under-aged conditions lead to permanent softening of the flow stress.     

Stress-Dependent Elastic Behaviour of a Titanium Alloy at Elevated Temperatures

In this study the influence of stress and temperature on the elastic modulus during fully-reversed low cycle fatigue of the titanium alloy Ti6242 is examined. The change of the elastic properties with stress manifests itself in a crescent-like shaped hysteresis loop of stress vs. plastic strain at very low amplitudes, i.e. below the technical yield stress. A quadratic extension of Hooke??s law with a second constant ??k?? is applied. The parameters are determined all along the unloading curve in tension and compression. The approach results in the alignment of the hysteresis loop so that they become vertical, i.e. the elastic strain is accurately described. The value and sign of ??k?? depend on whether the deformation occurs in tension or compression. Like the Young??s modulus E ₀, ??k?? also depends on temperature. At temperatures up to 550°C the values of ??k?? in tension and compression do not change during fatigue life. However, at 650°C thermally activated slip processes lead to changes of both, E ₀ and ??k??.     

Sn和Si含量对Al—Sn—Si合金室温压缩变形流变应力的影响

采用Gleeble-1500试验机，在室温和恒应变速率下，测定了Al-Sn-Si系合金压缩变形的流变应力曲线。结果表明，在Sn、Si含量分别为0－20和0－8wt．％的范围内，当Sn含量恒定时，流变应力随Si含量的增加而增加，而当Si含量恒定时，流变应力则随Sn含量的增加而略有降低；从Al-Sn-Si，Al-Si及Al-Sn 合金流变应力曲线的差异，分析了Sn和Si对合金塑性变形过程的影响机制。     

Artificial neural network prediction to the hot compressive deformation behavior of Al–Cu–Mg–Ag heat-resistant aluminum alloy

The behavior of the flow stress of Al-Cu-Mg-Ag heat-resistant aluminum alloys during hot compression deformation was studied by thermal simulation test. The temperature and the strain rate during hot compression were 340-500 °C, 0.001 s⁻¹ to 10 s⁻¹, respectively. Constitutive equations and an artificial neural network (ANN) model were developed for the analysis and simulation of the flow behavior of the Al-Cu-Mg-Ag alloys. The inputs of the model are temperature, strain rate and strain. The output of the model is the flow stress. Comparison between constitutive equations and ANN results shows that ANN model has a better prediction power than the constitutive equations.     

Ratchetting of viscoplastic material with cyclic softening,part 1: experiments on modified 9Cr–1Mo steel

Uniaxial and multiaxial ratchetting tests were conducted at temperatures between 200 and 600 °C on modified 9Cr–1Mo steel, which exhibits both viscoplastic and cyclic softening behavior. Anomalous behavior was observed in the stress-controlled uniaxial ratchetting tests; the material exhibited outstanding ratchetting in the tensile direction under zero mean stress. Under the uniaxial conditions, the ratchetting deformation significantly depended on the loading rate and hold time in addition to parameters such as the maximum stress and stress ratio. The uniaxial ratchetting was also accelerated to a great extent when cyclic deformation was given before the ratchetting tests. Under the multiaxial conditions, the ratchetting depended on the steady stress, cyclic strain range and strain rate. The ratchetting progressed faster as the steady stress or strain range became larger, or the strain rate became smaller, as expected. Monotonic compression tests were carried out to investigate the reason for the rachetting under no mean stress. Strain range change tests were also conducted to investigate the effect of strain range on the cyclic softening behavior of the material in detail.     

Uniaxial ratcheting and failure behaviors of two steels

The strain cyclic characteristics, ratcheting and failure behaviors of 25CDV4.11 steel and SS304 stainless steel were experimentally studied under uniaxial cyclic tests and at room temperature. The cyclic hardening/softening features of the materials were first observed under uniaxial strain cycling; and then the ratcheting and failure behaviors of the materials were researched in detail under cyclic stressing. The effects of stress amplitude and mean stress on the ratcheting and failure were discussed under uniaxial asymmetrical stress cycling. It is concluded that the ratcheting and failure behaviors of the materials depend greatly on the cyclic softening/hardening features of the materials and the stress values of cyclic loading. Some conclusions useful to understand the fatigue failure of the materials presented under asymmetrical cyclic stressing are obtained.     

YB-2航空有机玻璃的应变率和温度敏感性及其本构模型

为了理解和评价YB-2航空有机玻璃在极端环境下的动态力学性能,采用电子万能试验机和分离式Hopkinson压杆对YB-2航空有机玻璃在218~373 K温度范围、10-3~3 000 s-1应变率范围内的压缩力学行为进行了研究,得到了材料的应力应变曲线。结果表明:随着温度的升高,材料的流动应力逐渐减小而破坏应变呈现增大的趋势;温度相同时,材料的流动应力随应变率的增加而增大,破坏应变随应变率的增加而减小。随着应变率的提高,材料的应变软化效应更加剧烈。基于朱-王-唐(ZWT)本构模型,得到了考虑温度效应的本构参数。结果显示,在8%应变范围内,改进的考虑温度效应的本构模型可以较为理想地表征该材料的应力应变响应。     

The Effect of Temperature on Anisotropy Properties of an Aluminium Alloy

The temperature influence on the mechanical behaviour during plastic deformation of an AA5754-O aluminium alloy has been investigated by several experimental tests. First, monotonous tensile tests were carried out from room temperature up to 200°C with a classical tensile machine and with a less conventional testing apparatus involving the heating of the sample by Joule effect. With this second testing apparatus, the strain fields and tensile curves were obtained in function of temperature by means of a non-contacting optical 3D deformation measuring system. Moreover, shear tests were performed in the same temperature range. It is shown that the anisotropy coefficients are rather constant within this temperature range, with a relative variation less than 8%. For both tensile and shear tests, the stress levels are similar at the beginning of straining at room temperature and 150°C, except that the Portevin?CLe Chatelier (PLC) phenomenon disappears at elevated temperature, and then evolves differently. At 200°C, the stress level is clearly below whatever the deformation. In the framework of drawing process, the formability of this alloy at temperatures higher than 150°C seems to be improved.     

Balanced Biaxial Testing of Advanced High Strength Steels in Warm Conditions

The main purpose of the present work is to measure the stress–strain behavior under warm conditions (about 100 °C) of advanced high strength steel (AHSS) sheets up to large strains compared to uniaxial tension. The test equipment consists of two main parts, i.e., a hydraulic bulge tester and a heating device. A mechanical system is attached to the test equipment for measuring the membrane stress and thickness strain at the bulge pole. The stress–strain curves were measured for three kinds of AHSS sheets with the proposed test method for various initial temperatures (10, 50 and 100 °C). The proposed method does not provide isothermal stress–strain curves because the specimen temperature increases during the test due to the effect of deformation-induced heating. A numerical scheme using thermo-mechanical finite element (FE) simulations is suggested to deconvolute the isothermal stress–strain curves.     

The Effect of Grain Size on Deformation and Failure of Ti<Subscript>2</Subscript>AlC MAX Phase under Thermo-Mechanical Loading

An experimental investigation was performed to analyze the effects of grain size on the quasi-static and dynamic behavior of Ti₂AlC. High-density Ti₂AlC samples of three different grain sizes were densified using Spark Plasma Sintering and Pressureless sintering. A servo-hydraulic testing machine equipped with a vertical split furnace, and SiC pushrods, was used for the quasi-static experiments. Also, a Split Hopkinson Pressure Bar (SHPB) apparatus and an induction coil heating system were used for the dynamic experiments. A series of experiments were conducted at temperatures ranging from 25 °C to 1100 °C for strain rates of 10^?4 s^?1 and 400 s^?1. The results show that under quasi-static loading the specimens experience a brittle failure for temperatures below Brittle to Plastic Transition Temperature (BPTT) of 900–1000 °C and large deformation at temperatures above the BPTT. During dynamic experiments, the specimens exhibited brittle failure, with the failure transitioning from catastrophic failure at lower temperatures to graceful failure (softening while bearing load) at higher temperatures, and with the propensity for graceful failure increasing with increasing grain size. The compressive strengths of different grain sizes at a given temperature can be related to the grain length by a Hall-Petch type relation.     

Stress–strain behaviour of poly(ethylene terephthalate) (PET) during large plastic deformation by plane strain compression: the relation between stress–strain curve and thermal history, temperature and strain rate

This study presents an experimental investigation of the large plastic deformation of poly(ethylene terephthalate) (PET) submitted to plane strain compression. PET samples, obtained by injection moulding, annealed and non-annealed, were deformed using a specific compression device developed for this purpose. The obtained stress–strain curves at different temperatures and strain rates are useful for engineering applications and show a significant temperature dependence and a minor dependence on the strain rate. A softening temperature as a minimum temperature necessary to initiate deformation when a minimum, almost zero, stress is applied is introduced. This temperature, at the zero stress and strain limit, we denominate “Stress–Strain independent softening Temperature (T _SOF)”. The T _SOF values, 104 and 113°C for non-annealed and annealed PET, respectively, have been obtained using three different strain rates, indicating that the property is sensitive to the thermal history of the material.     

Development of temperature-compensated resistance strain gages for use to 700°C

This paper describes the development and evaluation of temperature-compensated resistance strain gages for use to 700°C (1292°F). These gages included single-element gage and double-element gages. The filament of single-element gages was fabricated from specially developed Fe?Cr?Al?V?Ti?Y alloy wire. When bonded to high-temperature Ni-based alloy GH30, the apparent strain from room temperature to 700°C was less than 1800 μm/m. Active grids of double-element gages were fabricated from specially developed Pt?W?Re?Ni alloy wire and Pt-W9.5 wire. The compensating elements were fabricated from Pt?Ir20 alloy wire. When bonded to different high-temperature alloys, by proper adjustment of the ballast resistor in series with the low-resistance Pt?Ir element, apparent strain in the related temperature range was less than 1000 μm/m. Equations to compute the allowable deviation of resistance of compensating element and of ballast resistor for the purpose of attainment of certain measurement accuracy were derived. This paper should be of particular interest to those involved in strain measurement at temperatures to 700°C.     

On modes and criteria of ABS melt failure in extension

Melt failure of a commercial ABS polymer in uniaxial extension over ranges of elongation rate ([(e)\dot] = 0.01 - 1.0 s ^{- 1}\dot \varepsilon = 0.01 - 1.0\,{\rm s}^{ - 1} ) and temperature (140-200 °C) was investigated. Four methods of experimental and numerical calculation for determination of modes and criteria of melt failure in uniaxial extension were investigated: 1) visual observation of necking; 2) visual observation of non-uniform flow during stress relaxation after cessation of steady elongation; 3) calculation of the Considère criterion from the measured elongational stress-strain curve; 4) numerical calculation of inflection point (‘C²/‘)²=0) from the tensile stress-strain curve. In addition, under higher Deborah number conditions the critical Hencky strains at Considère criterion were calculated using PSM model parameters (! and #) and were compared with those obtained from the measured elongational stress-strain curve. The relationship between these failure modes is discussed in terms of rheological properties of the polymer, putting emphasis on the relationship with the thermoforming process. The Considère criterion appears to be the most effective indicator of the non-uniform deformation of ABS melt in uniaxial extension under conditions where cohesive fracture does not occur. The rheological properties such as elongational viscosity, strain hardening and/or strain softening, and their temperature dependence play an important role in determining the growth and transition of melt failure of ABS polymer in uniaxial extension.     

金属铍的压缩变形行为

利用材料试验机及Hopkinson杆装置系统开展热等静压金属铍在不同温度下的静动态压缩力学行为研究,获得了温度、应变率对金属铍屈服强度和加工硬化行为的影响规律。结果表明:金属铍在压缩应力状态下呈现出良好的塑性,同时其力学性能具有显著的应变率敏感性与热软化效应,屈服强度和流动应力随应变率提高呈明显增大趋势,随着温度升高逐渐降低。同时,室温下其加工硬化行为随着应变增大表现为分段硬化特征,随温度升高则趋于理想塑性。最后,采用修正的Johnson-Cook本构模型对实验结果进行了拟合,模型计算结果与实验结果吻合较好。