Nitrogen/non-Newtonian fluid two-phase upward flow in non-circular microchannels

This paper presents experimental investigations on nitrogen/non-Newtonian fluid two-phase flow in vertical noncircular microchannels, which have square or triangular cross-section with the hydraulic diameters being D_h = 2.5, 2.886 and 0.866 mm, respectively, by visualization method. Three non-Newtonian aqueous solutions with typical rheological properties, i.e., 0.4% carboxymethyl cellulose (CMC), 0.2% polyacrylamide (PAM) and 0.2% xanthan gum (XG) are chosen as the working fluids. The common flow patterns are identified as slug flow, churn flow and annular flow. The dispersed bubble flow is only found in the case with nitrogen/CMC solution two-phase flow in the largest channel. A new flow pattern of nitrogen/PAM solution two-phase flow, named chained bubble/slug flow, is observed in all the test channels. The flow regime maps are also developed and the results show that the rheological properties of the non-Newtonian fluid have remarkable influence on the flow pattern transitions. The geometrical factors of the microchannel such as the cross-section shape and hydraulic diameter of the channel can also affect the flow regime map. Finally, the results obtained in this work are compared with the available flow pattern transitions.     

Visualization of flow boiling of liquid nitrogen in a vertical mini-tube

The flow boiling patterns of liquid nitrogen in a vertical mini-tube with an inner diameter of 1.931 mm are visualized with a high-speed digital camera. The superficial gas and liquid velocities are in the ranges of 0.01–26.5 m/s and 0.01–1.2 m/s, respectively. Four typical flow patterns, namely, bubbly, slug, churn and annular flow are observed. Some interesting scenes about the entrainment and liquid droplet deposition in the churn and annular flow, and the flow reversal with the indication of negative pressure drop, are also presented. Based on the visualization, the two-phase flow regime maps are obtained. Compared with the flow regime maps for gas–water flow in tubes with similar hydraulic diameters, the region of slug flow in the present study reduces significantly. Correspondingly, the transition boundary from the bubbly flow to slug flow shifts to higher superficial gas velocity, and that of churn to annular flow moves to lower superficial gas velocity. Moreover, time-averaged void fraction is calculated by quantitative image-digitizing technique and compared with various prediction models. Finally, three kinds of oscillations with long-period and large-amplitude are found, possible explanation for the oscillations is given by comparing the instantaneous flow images with the data of pressure, mass flux and temperature recorded synchronously.     

Flow regime transition criteria for two-phase flow at reduced gravity conditions

Flow regime transition criteria are of practical importance for two-phase flow analyses at reduced gravity conditions. Here, flow regime transition criteria which take the frictional pressure loss effect into account were studied in detail. Criteria at reduced gravity conditions were developed by extending an existing model from normal gravity to reduced gravity conditions. A comparison of the newly developed flow regime transition criteria model with various experimental datasets taken at microgravity conditions showed satisfactory agreement. Sample computations of the model were performed at various gravity conditions, such as 0.196, 1.62, 3.71 and 9.81 m/s² corresponding to micro-gravity and lunar, Martian and Earth surface gravity, respectively. It was found that the effect of gravity on bubbly–slug and slug–annular (churn) transitions in a two-phase flow system was more pronounced at low liquid flow conditions, whereas the gravity effect could be ignored at high mixture volumetric flux conditions. While for the annular flow transitions due to flow reversal and onset of droplet entrainment, higher superficial gas velocity was obtained at higher gravity level.     

Studies on two-phase co-current air/non-Newtonian shear-thinning fluid flows in inclined smooth pipes

In this work, co-current flow characteristics of air/non-Newtonian liquid systems in inclined smooth pipes are studied experimentally and theoretically using transparent tubes of 20, 40 and 60 mm in diameter. Each tube includes two 10 m long pipe branches connected by a U-bend that is capable of being inclined to any angle, from a completely horizontal to a fully vertical position. The flow rate of each phase is varied over a wide range. The studied flow phenomena are bubbly flow, stratified flow, plug flow, slug flow, churn flow and annular flow. These are observed and recorded by a high-speed camera over a wide range of operating conditions. The effects of the liquid phase properties, the inclination angle and the pipe diameter on two-phase flow characteristics are systematically studied. The Heywood–Charles model for horizontal flow was modified to accommodate stratified flow in inclined pipes, taking into account the average void fraction and pressure drop of the mixture flow of a gas/non-Newtonian liquid. The pressure drop gradient model of Taitel and Barnea for a gas/Newtonian liquid slug flow was extended to include liquids possessing shear-thinning flow behaviour in inclined pipes. The comparison of the predicted values with the experimental data shows that the models presented here provide a reasonable estimate of the average void fraction and the corresponding pressure drop for the mixture flow of a gas/non-Newtonian liquid.     

On two-phase flow patterns and transition criteria in aqueous methanol and CO2 mixtures in adiabatic,rectangular microchannels

This paper presents flow map investigations of adiabatic two-phase flow in square cross-sectioned, 200 μm deep microchannels fabricated in silicon, employing laser induced fluorescence microscopy. The influence of surface tension and nozzle geometry on the flow pattern transition was investigated using two nozzle widths (orifices of 30 μm and 50 μm, respectively) and methanol–water solutions with CO₂ as the gas phase. It was found and quantified that smaller nozzle geometries and smaller liquid surface tension promote the propagation of capillary gas bubbles at lower superficial gas and liquid velocities. Within the measurement domain of superficial gas (0.01–0.625 m/s) and liquid (0.0005–0.5000 m/s) velocities, we observed dispersed bubbly, regularly ordered bubbly, wedging, slug and annular flows, thus extending the experimental knowledge base to smaller superficial liquid velocities by almost two orders of magnitude. With the help of the flow maps presented herein, we were able to characterize the observed regularly ordered bubbly flow as the transition regime between dispersed bubbly and wedging flow. The results of the present investigation are of direct relevance to the operation of small-scale direct methanol fuel cells.     

An appraisal of liquid–liquid slug flow in different pipe orientations

Gas–liquid slug flow occurs over a wide range of phase flow rates and in a variety of practical applications during gas–liquid two-phase flows. The range of slug flow increases further in narrow pipes (<0.0254 m), undulated pipelines, riser tube, etc. On the other hand, the past literature shows that slug flow is rarely observed for liquid–liquid cases. In the present study, an interest was felt to investigate whether liquid–liquid slug flow occurs in situations known for excessive slugging in gas–liquid cases. For this, experiments have been performed in narrow (0.012 m ID) vertical and horizontal pipes and an undulated pipeline of 0.0254 m internal diameter where the V-shaped undulation comprises of an uphill and a downhill section between two horizontal pipes. The studies have been performed for both peak and valley orientation of the undulation. Kerosene and water have been selected as the test fluids and the optical probe technique has been used to supplement visual observations especially at higher flow rates. The studies have revealed the existence of the slug flow pattern over a wide range of phase flow rates in all the three geometries. Interestingly, it has been noted that the introduction of an undulation induces flow patterns which bear a closer resemblance to gas–liquid flows as compared to liquid–liquid flows through a horizontal pipe of 0.0254 m diameter.     

Experimental study on axial development of liquid film in vertical upward annular two-phase flow

Accurate measurements of the interfacial wave structure of upward annular two-phase flow in a vertical pipe were performed using a laser focus displacement meter (LFD). The purpose of this study was to clarify the effectiveness of the LFD for obtaining detailed information on the interfacial displacement of a liquid film in annular two-phase flow and to investigate the effect of axial distance from the air–water inlet on the phenomena. Adiabatic upward annular air–water flow experiments were conducted using a 3 m long, 11 mm ID pipe. Measurements of interfacial waves were conducted at 21 axial locations, spaced 110 mm apart in the pipe. The axial distances from the inlet (z) normalized by the pipe diameter (D) varied over z/D = 50–250. Data were collected for predetermined gas and liquid flow conditions and for Reynolds numbers ranging from Re_G = 31,800 to 98,300 for the gas phase and Re_L = 1050 to 9430 for the liquid phase. Using the LFD, we obtained such local properties as the minimum thickness, maximum thickness, and passing frequency of the waves. The maximum film thickness and passing frequency of disturbance waves decreased gradually, with some oscillations, as flow developed. The flow development, i.e., decreasing film thickness and passing frequency, persisted until the end of the pipe, which means that the flow might never reach the fully developed state. The minimum film thickness decreased with flow development and with increasing gas flow rate. These results are discussed, taking into account the buffer layer calculated from Karman’s three-layer model. A correlation is proposed between the minimum film thickness obtained in relation to the interfacial shear stress and the Reynolds number of the liquid.     

Flow patterns of n-hexadecane–CO2 liquid–liquid two-phase flow in vertical pipes under high pressure

To promote a better understanding of liquid–liquid two-phase flow behavior, particularly under high pressure, flow patterns of n-hexadecane–CO₂ liquid–liquid two-phase upward flow in vertical stainless steel pipes were experimentally investigated. Observations were made in two 0.0015 m I.D. pipes of different lengths (0.068 m and 0.5 m) under high pressure varying from 10.3 to 29.6 MPa using a high pressure visualization system. The total flow rate was fixed at 2.0 × 10⁻⁶ m³/min, while the flow rate ratio (φ) varied from 0.05 to 19. Bubbly flow, plug flow, slug flow, annular flow, and near-one-phase flow regions were found in both pipes, while stratified flow was observed only in the 0.068 m pipe. Flow pattern maps were constructed in the flow rate ratio versus pressure graph, which demonstrates significant impacts of flow rate ratio, pipe length, and pressure on flow patterns. These impacts are discussed in detail. To the authors’ best knowledge, this work is the first attempt to observe complex liquid–liquid two-phase flow behavior with flow pattern transitions under high pressure, and contributes to a better understanding of liquid–liquid two-phase flow behavior.     

The split of vertical annular flow at a large diameter T junction

Measurements and observations have been made of the split of gas—liquid flow at a T junction where the main pipe was vertical and the side arm horizontal. All three pipes connecting to the junction were of 0.125 m dia. The gas and liquid flow rates were chosen to ensure annular flow in the inlet pipe. The resulting data have been compared with existing models.     

Equal quality distribution of gas–liquid two-phase flow by partial separation method

This paper proposes a new method for equal quality distribution of gas–liquid two-phase flow by partial separate-phase distribution with a dual-header distributor. The upper and liquid (lower) headers are interconnected with five vertical downward arms. A gas–liquid two-phase mixture enters the distributor from the upper header where most of the liquid of the mixture is removed through the downward arms into the liquid header. Hence, firstly, the remaining gas-rich fluid can be uniformly distributed into the outlet branches, and then secondly, the liquid collected in the liquid header can be uniformly re-distributed into the individual outlet branches. Because both distribution processes are conducted in the condition of single or near single-phase flow, mal-distribution of the two-phase flow is essentially eliminated, and a satisfactory equal quality distribution of gas–liquid two-phase flow is reached. Experiments were conducted in an air–water two-phase flow test loop. The inner diameter of the inlet pipe was 60 mm, the superficial velocity ranges of gas and liquid were 3–32 m/s and 0.02–0.17 m/s respectively, and the quality ranged from 0.02 to 0.44. The flow pattern in the inlet pipe included stratified flow, wavy stratified, slug flow, and annular flow. The experimental results showed that this new method could significantly improve the distribution performance of the two-phase flow. The maximum quality deviation between each outlet branch and the inlet pipe is less than ±1% under the conditions of stratified, wavy stratified and slug flows in the upper header, and less than ±5% in annular flow.     

Viscous oil–water flows in a microchannel initially saturated with oil: Flow patterns and pressure drop characteristics

Immiscible viscous liquid–liquid two-phase flow patterns and pressure drop characteristics in a circular microchannel have been investigated. Water and silicone oil with a dynamic viscosity of 863 mPa s were injected into a fused silica microchannel with an inner diameter of 250 μm. As the microchannel was initially filled with the silicone oil, an oil film was found to always form and remain on the microchannel wall. Different flow patterns were observed and classified over a wide range of water and oil flow rates. A flow pattern map is presented in terms of Re, Ca, and We numbers. Two-phase pressure drop data have also been collected and analyzed to develop a simple correlation for slug, annular and annular-droplet flow patterns in terms of superficial water and oil velocities.     

Gas/shear-thinning liquid flows through pipes: Modeling and experiments

In chemical and oil industry gas/shear-thinning liquid two-phase flows are frequently encountered. In this work, we investigate experimentally the flow characteristics of air/shear-thinning liquid systems in horizontal and slightly inclined smooth pipes. The experiments are performed in a 9-m-long glass pipe using air and three different carboxymethyl cellulose (CMC) solutions as test fluids. Flow pattern maps are built by visual observation using a high-speed camera. The observed flow patterns are stratified, plug, and slug flow. The effects of the pipe inclination and the rheology of the shear-thinning fluid in terms of flow pattern maps are presented. The predicted existence region of the stratified flow regime is compared with the experimental observation showing a good agreement. A mechanistic model valid for air/power-law slug flow is proposed and model predictions are compared to the experimental data showing a good agreement. Slug flow characteristics are investigated by the analysis of the signals of a capacitance probe: slug velocity, slug frequency, and slug lengths are measured. A new correlation for the slug frequency is proposed and the results are promising.     

Flow regime transition criteria for two-phase flow in a vertical annulus

In this work, a new flow regime transition model is proposed for two-phase flows in a vertical annulus. Following previous works, the flow regimes considered are bubbly (B), slug (S) or cap-slug (CS), churn (C) and annular (A). The B to CS transition is modeled using the maximum bubble package criteria of small bubbles. The S to C transition takes place for small annulus perimeter flow channels and it is assumed to occur when the mean void fraction over the entire region exceeds that over the slug–bubble section. If the annulus perimeter is larger that the distorted bubble limit the cap-slug flow regime will be considered since in these conditions it is not possible to distinguish between cap and partial-slug bubbles. The CS to C transition is modeled using the maximum bubble package criteria. However, this transition considers the coalescence of cap and spherical bubbles in order to take into account the flow channel geometry. Finally, the C to A transition is modeled assuming two different mechanisms, (a) flow reversal in the liquid film section along large bubbles; (b) destruction on liquid slugs or large waves by entrainment or deformation. In the S to C and C to A flow regime transitions the annulus flow channel is considered as a rectangular flow channel with no side walls. In all the modeled transitions the drift-flux model is used to obtain the final correlations. The final equations for every flow regime transition are easy to be implemented in computational codes and not experimental input is needed. The prediction accuracy of the newly developed model has been checked against air–water as well as boiling flow regime maps. In all the cases, the new developed model shows better predicting capabilities than the existing correlations most used in literature.     

Numerical modeling and experimental investigation of gas–liquid slug formation in a microchannel T-junction

Gas–liquid two-phase flow in a microfluidic T-junction with nearly square microchannels of 113 μm hydraulic diameter was investigated experimentally and numerically. Air and water superficial velocities were 0.018–0.791 m/s and 0.042–0.757 m/s, respectively. Three-dimensional modeling was performed with computational fluid dynamics (CFD) software FLUENT and the volume of fluid (VOF) model. Slug flow (snapping/breaking/jetting) and stratified flow were observed experimentally. Numerically predicted void fraction followed a linear relationship with the homogeneous void fraction, while experimental values depended on the superficial velocity ratio U_G/U_L. Higher experimental velocity slip caused by gas inlet pressure build-up and oscillation caused deviation from numerical predictions. Velocity slip was found to depend on the cross-sectional area coverage of the gas slug, the formation of a liquid film and the presence of liquid at the channel corners. Numerical modeling was found to require improvement to treat the contact angle and contact line slip, and could benefit from the use of a dynamic boundary condition to simulate the compressible gas phase inlet reservoir.     

On the role of droplets in cocurrent annular and churn-annular pipe flow

Decreasing the gas flow-rate in an initially vertical upward annular dispersed pipe-flow, will eventually lead to a down-flow of liquid. The onset of this down-flow has been related in the literature to the presence of the dispersed phase and the instability of the liquid film. Here we investigate how the dispersed-phase may influence the down-flow, performing detailed PDA-measurements in a 5 cm vertical air–water annular-flow. It is shown that the dispersed-phase does not cause the liquid down-flow, but that it delays the onset of liquid down-flow. In cocurrent annular flow the dispersed phase seems to stabilise the film flow, whereas in churn-annular flow the opposite seems to be true.     

Two-phase stratified flow splitting at a T-jun

The objective of this study is to investigate, experimentally and theoretically, two-phase splitting under stratified wavy flow conditions at a regular horizontal T -junction with an inclined branch arm.

Experimental data have been acquired with the side arm at horizontal conditions, downward inclination angles of −5, −10, −25, −40 and −60°, and upward inclinations of 1, 5, 10, 20, and 35° from the horizontal. The data reveal that gravity forces have a significant effect on the flow splitting. For downward inclination of the side arm more liquid is diverted into the branch arm, as compared to the case in which the side arm was horizontal. All the liquid was found to be diverted into the branch arm when the branch arm inclination was increased to −60°. For upward inclination angles a significant amount of the inlet gas has to be diverted into the side arm in order to get any liquid to flow into that arm. However, once liquid has started flowing, not much more additional gas has to be diverted into the side arm to get all of the liquid to flow into the branch. At 35° almost all the gas has to be diverted for any liquid flow into the branch.

A mechanistic model has been developed for the prediction of the splitting phenomenon for both the horizontal and the downward orientations of the side arm. The model is based on the momentum equations applied for the separation streamlines of the gas phase and the liquid phase. Very good agreement is observed between the prediction of the model and the data acquired for all the cases.     

Refrigerant distribution in a parallel flow heat exchanger having vertical headers and heated horizontal tubes

Refrigerant R-410a flow distribution is experimentally studied in a test section simulating a parallel flow heat exchanger having vertical headers with two pass configuration. Tubes are heated to yield a test section outlet superheat of 5 °C with inlet quality of 0.3. Mass flux is varied from 50 kg/m² s to 70 kg/m² s. Effects of inlet and outlet locations are investigated in a search for an optimum configuration. Results show that, significant liquid flows through bottom channels, and less liquid is supplied to top channels. As for the inlet location, better flow distribution (pressure drop as well) is obtained for top inlet as compared with middle inlet. As for the outlet location, top or bottom outlet is better than middle outlet. Correlations are developed for the fraction of liquid or gas taken off by downstream channel as a function of header gas Reynolds number at immediate upstream. The correlations may be used to predict the liquid or gas distribution in a parallel flow heat exchanger having vertical headers. A novel thermal performance evaluation method, which accounts for tube-side flow mal-distribution is proposed.     

Effect of diameter on two-phase pressure drop in narrow tubes

The effect of tube diameter on two-phase frictional pressure drop was investigated in circular tubes with inner diameters of 0.6, 1.2, 1.7, 2.6 and 3.4 mm using air and water. The gas and liquid superficial velocity ranges were 0.01-50 m/s and 0.01-3 m/s, respectively. The gas and liquid flow rates were measured and the two-phase flow pattern images were recorded using high-speed CMOS camera. Unique flow patterns were observed for smaller tube diameters. Pressure drop was measured and compared with various existing models such as homogeneous model and Lockhart-Martinelli model. It appears that the dominant effect of surface tension shrinking the flow stratification in the annular regime is important. It was found that existing models are inadequate in predicting the pressure drop for all the flow regimes visualized. Based on the analysis of present experimental frictional pressure drop data a correlation is proposed for predicting Chisholm parameter “C” in slug annular flow pattern. For all other flow regimes Chisholm’s original correlation appears to be adequate except the bubbly flow regime where homogeneous model works well. The modification results in overall mean deviation of pressure drop within 25% for all tube diameters considered. This approach of flow regime based modification of liquid gas interaction parameter appears to be the key to pressure drop prediction in narrow tubes.