Multi-core orthogonal fluxgate sensor

A multi-core orthogonal fluxgate sensor is presented, in which the sensing element is formed by multiple insulated thin-wires of a soft ferromagnetic material. Experiments were conducted to investigate the characteristics of the sensor. The results showed that the sensor sensitivity increased exponentially with increasing the number of cores in the sensing element. Such an increase was neither due to increase in the excitation current passing through the sensing element because the number of cores was increased, nor due to the increase of the ferromagnetic material in the sensing element. The results further showed that the sensitivity increases with increasing the number of cores exponentially only if the multiple cores of the sensing element are closely packed, and that there is a resonance in the sensing output corresponding to an external field, which becomes significant as the number of cores reaches a certain large value and varies in its corresponding external magnetic field with the frequency of the excitation current. All the results indicated that in multi-core orthogonal fluxgate sensor, driven by the high frequency of the excitation current passing through the multiple cores, there is a dynamic magnetic interaction between the cores in the sensing element, which increases the sensitivity.     

Electrodeposition and characteristics of Ni80Fe20/Cu composite wires

Electrodeposited Ni₈₀Fe₂₀/Cu composite wire has significant advantages over amorphous wire as sensing element for weak magnetic field sensors, such as orthogonal fluxgate sensors, due to its non-ferromagnetic and conductive core structure. In this study, the key processing parameters are investigated, including electrodeposition current density, duty cycle, electrolyte solution, pH value, applied magnetic field, effect of seeded layers, and post annealing.     

高斯噪声和弱正弦信号驱动的时间差型磁通门传感器

提出了一种利用高斯噪声和弱正弦信号共同驱动的新型时间差型磁通门传感器.根据软磁材料双稳态特性及其Fokker-Planck方程推导了跃迁率的表达式.利用数值仿真的方法,研究了跃迁率和外磁场、激励磁场、噪声强度之间的关系.通过将周期变化的跃迁率信号转换为方波信号,建立了方波高低电平时间差与外磁场之间的关系,并推导了传感器灵敏度的表达式.研究表明,在一定的偏置磁场下,传感器灵敏度与激励磁场的幅值以及频率成反比,量程和激励磁场的幅值成正比.对所设计±10.7A/m量程的传感器样机进行了测试,传感器最小灵敏度为9.8696 ms/(A/m),可用于准静态微弱磁场的检测.     

Peculiarities of permalloy thin film microcore hysteretic magnetization process in high space resolution fluxgate device

Magnetization processes of the sectioned thin film permalloy core were examined in relation with its geometrical dimensions using magnetooptical Kerr technique and ferrofluid observation. It is shown quantitatively the intermediate case between Stoner–Wohlfarth and zero internal field contradicting models takes place. Ferrofluid investigation had shown the stable quasi-saturated state with closing domain structures at permalloy bar edges. Magnetization reversal occurs by hysteretic manner but the hysteresis loop parameters are reproducible and depend strongly upon core geometry. Hysteresis is characterized by parallelogram form with clear critical field and loop slope depending on bars dimensions and their mutual position in array. Loop shape approaches the rectangular form and critical field increases if bar thickness t, width w and bar density in array are decreased. The critical field value H_cr is defined by demagnetizing field at bar edges while the saturation field H_s depends only on width w at of a bar in array. Variation of the bar form or shift of every second bar in array possesses to increase the core thickness to enhance the stray field without increase of the saturating exciting current. The core described can be used with magnetooptical garnet film or Hall sensor in fluxgate regime for magnetic field measurement with space resolution 10–100 mcm.     

Coil-less fluxgate effect in (Co0.94Fe0.06)72.5Si12.5B15 amorphous wires

In this study, the coil-less fluxgate properties of the as-cast and annealed amorphous wires with the composition (Co_0.94Fe_0.06)_72.5Si_12.5B₁₅ were investigated. As its name implies, a coil-less fluxgate is a new type of magnetic-field sensor without a coil. When the wire is periodically saturated in a magnetic field in the circumferential direction with a 30 kHz, 62 mA driving current under a 16.5π rad/m torsional strain, there is a linear variation in the second harmonic of the voltage from the wire ends as a function of the applied external DC magnetic field along the length of the wire.Current-stress annealing of each sample improved the sensitivity of the coil-less fluxgate sensor. This is the first time that it has been shown that a linear change in the output of the coil-less fluxgate sensor can be obtained using torsion annealed wire without the necessity of twisting the wire during measurement. We showed that the linear operating range of the sensor can be increased by increasing the demagnetization factor in the sensing direction, so that the coil-less fluxgate sensor can be miniaturised just by reducing the wire length.     

Effects of helical anisotropy on nonlinear voltage response in amorphous wires

The nonlinear voltage response in soft magnetic amorphous wires exciting by an alternating current is studied. The frequency spectrum of the voltage in the pick-up coil wound around the wire with a helical anisotropy is found in the framework of a model based on quasi-static Stoner−Wohlfarth magnetization reversal. The effect of a deviation of the anisotropy axis from the azimuthal direction on the field dependences of amplitudes of voltage harmonics is analyzed. It is shown that the field sensitivity of even harmonics increases with the anisotropy axis deviation angle. The current amplitude range to obtain a maximal field sensitivity of the second harmonic is found. The influence of the skin effect on the frequency spectrum of the pick-up coil voltage is discussed. The results obtained may be of importance for the development of sensors of a weak magnetic field.     

磁致伸缩材料弱磁场响应特性的实验研究

针对磁致伸缩材料在弱磁场传感器领域的应用需要,采用迈克耳逊干涉原理实验测量了零应力条件下Tb-Dy-Fe材料和Fe-Ga合金的磁场响应灵敏度,以及不同应力下Fe-Ga合金的磁场响应特性和温度响应特性.实验结果表明：在零应力,外加磁场16 mT条件下,Fe-Ga合金的磁场响应灵敏度远高于Tb-Dy-Fe材料,更合适作为弱磁场传感器敏感材料;同时,在1.2 MPa预应力和26 mT偏置磁场下,Fe-Ga合金材料具有较好的磁场响应灵敏度和较大的饱和磁致伸缩系数,因而处在最佳工作状态.所得到的材料的磁场和温度响应曲线可作为弱磁场传感器参量设计的参考依据.     

Micromagnetic simulation of magnetic vortex cores in circular permalloy disks: Switching behavior in external magnetic field

Switching behaviors of magnetic vortex cores under external magnetic field in submicron circular permalloy disks have been systematically studied by using micromagnetic simulations. Simulation results show that the vortex core is stable in out-of-plane field even when it is located at the edge of the disk. The out-of-plane switching field H_sw is strongly dependent on the thickness of the disk. The core polarity and the vortex chirality can be modulated simultaneously on purpose by using a tilted field far smaller than the out-of-plane switching field H_sw. Moreover, it is found that the core polarities in asymmetric disks do not follow the direction of the z projection of the external saturation field.     

Characterization of magnetic core-shell nanoparticles by fluxgate magnetorelaxometry, ac susceptibility, transmission electron microscopy and photon correlation spectroscopy—A comparative study

We have compared the structure parameters of magnetic core-shell nanoparticles determined from fluxgate magnetorelaxometry measurements applying the moment superposition model with the results from other methods. For the characterization of the magnetic cores, the nanoparticles are immobilized by freeze-drying. The core size distribution estimated for superparamagnetic Fe₃O₄ magnetic nanoparticles (MNPs) with polyacrylic acid shell agrees well with that from transmission electron microscopy measurements. The distribution of hydrodynamic diameters of nanoparticle suspensions estimated from magnetorelaxometry measurements is in good agreement with that obtained from ac susceptibility and photon correlation spectroscopy measurements. Advantages of magnetorelaxometry compared to the other two integral techniques are that it is fast and the signal is less dominated by larger particles.     

环形激光弱磁传感器误差分析

本文从理论上分析了环形激光弱磁传感器主要误差因素并提出了若干克服这些因素的方法。这些误差因素是:大尺寸的法拉第室引入的噪声,磁光材料的费尔德常数的温度系数,塞曼效应的混入、朗谬尔效应等。     

Efficient compensation of low-frequency magnetic field disturbances in NMR with fluxgate sensors

A simple stabilization scheme of B(0) magnetic field fluctuations is described. The method is based on external measurements of time dependent magnetic field fluctuations by fluxgate sensors and generation of a compensating correction current in a coil mounted directly on an NMR magnet. It is shown that such an approach efficiently eliminates relatively slow magnetic field variations with frequency up to approximately 100 Hz. In combination with a standard (2)H field-frequency lock system, the method enables acquisition of reproducible lineshapes and dramatically improves overall performance of a high resolution NMR spectrometer. The presented solution might substitute for the internal lock system in these case where deuterium lock is not available.     

基于光子晶体光纤交叉敏感分离的磁场温度传感研究

提出了一种基于定向耦合效应和表面等离子共振效应的交叉敏感分离的磁场温度传感结构.在光子晶体光纤的一个特定空气孔中填充磁流体,利用磁流体的磁光效应和定向耦合效应形成磁场传感通道;在垂直方向的另一空气孔的内壁镀金纳米薄膜并填充甲苯液体,利用甲苯的温敏效应和表面等离子共振效应形成温度传感通道.对应输出谱出现两个损耗峰,测量损耗峰位置可以间接测出磁场强度和温度变化.通过理论计算()和结构优化,在90—270 Oe1 Oe=10~3/(4π) A/m范围内,磁场强度的灵敏度最高可达1.16 nm/Oe;在25—60?C范围内,温度的灵敏度可达-9.07 nm/?C.虽然填充的两种液体的折射率都受环境温度的影响,但通过建立灵敏度系数矩阵,可以消除磁场强度与温度的交叉敏感,实现磁场温度双参量的高灵敏度检测.     

基于酒精与磁流体填充的单模-空芯-单模光纤结构温度磁场双参数传感器

提出了一种基于空芯光纤模间干涉原理的环境温度和磁场双参数传感器,为了使光入射进空芯光纤壁中,将空芯光纤与单模光纤错位熔接,传感部分用毛细玻璃管封装,空芯光纤内外分别填充酒精和磁流体.除了光纤材料的热光效应和热膨胀效应外,环境温度变化会引起两种溶液折射率的变化,而磁场变化仅引起空芯光纤外的磁流体折射率变化.理论计算可知空芯光纤壁中可支持多个模式传输并相互干涉,各模式传输相位对内外溶液折射率变化灵敏程度不同.因此,干涉谱中两个含有不同模式成分的波谷,即波谷1和波谷2,它们的漂移可以作为指示信号,通过建立敏感矩阵可同时解调出周围环境温度与磁场的变化.实验中,在28—58℃范围内,温度传感灵敏度可达-468 pm/℃;在0—169 Oe范围内磁场传感灵敏度可达82 pm/Oe.该传感器具有高灵敏度与高机械强度,并且能够实现温度与磁场的同时测量,有效消除了温度波动对磁场测量信号的干扰.     

轴对称磁透镜设计

以中国科学院近代物理研究所正在研制的轴对称磁透镜为例,设计了两种结构的轴对称磁透镜:带屏蔽铁壳的螺线管透镜和极靴形状为锥形的Glaser透镜。带屏蔽铁壳的螺线管透镜产生的轴对称磁场比较均匀,而极靴形状为锥形的Glaser透镜产生的轴对称磁场比较集中。分别采用了两种物理模型计算磁场,同时应用有限元分析软件ANSYS进行数值模拟,最后从物理和工程角度对这两种透镜作了全面比较,得出带屏蔽铁壳的螺线管透镜结构更符合设计要求。     

基于磁通门和时域数字鉴频的磁场锁定系统

永磁型磁共振仪器的磁体易受温度和其他环境磁场干扰,造成主磁场波动,进而影响仪器测量的重复性和准确性.本文讨论了两种解决磁场波动的锁定方法：一方面,通过磁通门传感器对环境波动引起的瞬态磁场进行高灵敏探测,然后采用现场可编程门阵列进行实时处理并计算磁场补偿量;另一方面,针对环境温度变化引起的缓慢磁场偏移,则采用时域数字鉴频锁场方法,在对锁样品进行射频激发后,将磁共振信号通过混频变换到较低的频率范围,再转换为方波,然后直接送入现场可编程门阵列进行周期测量,并计算磁场补偿量.将两种方法获得的磁场补偿量叠加后,再转换为电流信号驱动安装在磁体上的B₀补偿线圈,并研制了一套磁场锁定系统,以实现对磁场的锁定. 在0.5 T食品快检磁共振分析仪上进行测试验证,结果显示当受到瞬态干扰时,可将磁场稳定在±4 Hz（对应磁场为±0.093 9 μT）范围内,同时也可以精准测量温度造成的磁场偏移,该结果验证了本文磁场锁定方法的可行性.     

Magnetic nanofibers with core (Fe3O4 nanoparticle suspension)/sheath (poly ethylene terephthalate) structure fabricated by coaxial electrospinning

One-dimensional magnetic nanostructures have recently attracted much attention because of their intriguing properties that are not realized by their bulk or particle form. These nanostructures are potentially useful for the application to ultrahigh-density data storages, sensors and bulletproof vest. The magnetic particles in magnetic nanofibers of blend types cannot fully align along the external magnetic field because magnetic particles are arrested in solid polymer matrix. To improve the mobility of magnetic particles, we used magneto-rheological fluid (MRF), which has the good mobility and dispersibility. Superparamagnetic core/sheath composite nanofibers were obtained with MRF and poly (ethylene terephthalate) (PET) solution via a coaxial electrospinning technique. Coaxial electrospinning is suited for fabricating core/sheath nanofibers encapsulating MRF materials within a polymer sheath. The magnetic nanoparticles in MRF were dispersed within core part of the nanofibers. The core/sheath magnetic composite nanofibers exhibited superparamagnetic behavior at room temperature and the magnetic nanoparticles in MRF well responded to an applied magnetic field. Also, the mechanical properties of the nanofiber were improved in the magnetic field. This study aimed to fabricate core/sheath magnetic composite nanofibers using coaxial electrospinning and characterize the magnetic as well as mechanical properties of composite nanofibers.     

Detection of magnetic nanoparticles with magnetoencephalography

Superconducting quantum interference devices (SQUIDs) have been widely utilized in biomedical applications due to their extremely high sensitivity to magnetic signals. The present study explores the feasibility of a new type of nanotechnology-based imaging method using standard clinical magnetoencephalographic (MEG) systems equipped with SQUID sensors. Previous studies have shown that biological targets labeled with non-toxic, magnetized nanoparticles can be imaged by measuring the magnetic field generated by these particles. In this work, we demonstrate that (1) the magnetic signals from certain nanoparticles can be detected without magnetization using standard clinical MEG, (2) for some types of nanoparticles, only bound particles produce detectable signals, and (3) the magnetic field of particles several hours after magnetization is significantly stronger than that of un-magnetized particles. These findings hold promise in facilitating the potential application of magnetic nanoparticles to in vivo tumor imaging. The minimum amount of nanoparticles that produce detectable signals is predicted by theoretical modeling and computer simulation.     

快脉冲大尺寸非晶态磁芯研究进展

通过对带绕非晶态软磁合金磁芯片间绝缘技术的几种方法、磁场热处理技术以及绝缘封装技术的研究,实现了非晶态磁芯片间0.6~1.0μm厚SiO2绝缘涂层以及片间击穿电压不低于120 V直流;非晶态磁芯纵磁热处理剩磁比大于0.90,横磁热处理剩磁比小于0.20,且绝缘封装前后磁芯磁性能变化小于5%。通过对快脉冲条件下带绝缘涂层大尺寸带绕非晶态软磁合金磁芯的研究,测试获得了试验磁芯的脉冲磁导率以及磁通跳变,其中1 000 mm级铁基非晶磁芯在脉冲间隔500 ns、脉冲宽度120 ns三脉冲串条件下,磁通跳变达到了2.86 T。     

Strain imaging of a perpendicular recording head in a Hard Disk Drive

Imaging of magnetic-field-induced strains using scanning probe microscopy enables us to observe magnetic domain structures and magnetic force distributions. This method has an ability of observing magnetic structures in deep portions along with surface structures. We observed an air-bearing surface of a perpendicular recording head in a hard disk drive in large areas including the whole yokes, and investigated characteristics of the magnetic poles and layers subjected to magnetic fields produced by writing coil currents. Attractive forces independent of the field directions acted between the upper and lower yokes made by soft material, which generated surface displacements in the ABS. The signals were second-harmonic oscillations for alternating currents without a dc bias, and the amplitude images represented the field distribution. Meanwhile, fixed magnetic charges in both ends of the read sensor, which were produced by the hard-bias film, were subjected to the fields. The fixed charges, which hardly changed by the fields, lead to strains depending on the field directions, and generated specific contrasts of one pair of bright-dark spots in the strain images. In the absence of surface underlayer, the fields by the writing coil broke into the read sensor sandwiched by the shield layers.     

Recent advances in studies of magnetically soft amorphous microwires

In this paper, we present the giant magneto-impedance (GMI) effect (real part of longitudinal impedance, Z, and of the off-diagonal impedance) and hysteretic magnetic properties of amorphous glass-coated microwires with different compositions possessing nearly zero, positive and negative magnetostriction constant and metallic nucleus diameter ranging between 6 and 16 μm. Enhanced soft magnetic properties (low coercivity of about 4 A/m) and high-GMI effect have been observed in Co-rich microwires with vanishing magnetostriction constant. The magnetic anisotropy field of these microwires depends on the ratio between metallic diameter, d and total microwires diameter, D. Stress-sensitive magnetic properties have been obtained in Fe-rich microwires after stress annealing: hysteresis loop stress-annealed (SA) microwires drastically changes under applied stress. A variety of hysteresis loops with different hysteresis loops can be obtained in Fe-rich microwires changing the conditions (time and/or temperature) of the stress annealing. The obtained results allow us to tailor the microwire magnetic properties for magnetic sensors applications through selection of their composition and/or geometry and by thermal treatment.