共查询到20条相似文献,搜索用时 46 毫秒
1.
Crystallography Reports - Two coordination polymers, {[L1Zn(adc)]2⋅5H2O}n (1), {[L1Cd(adc)]2⋅2.75H2O}n (2) (L1 = bis(4-(1H-imidazol-1-yl)phenyl)methanone, H2adc =... 相似文献
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Crystallography Reports - Two novel complexes, {[L1Ni(ipa)(H2O)]2(DMF)}n (1) and {[L1Zn(pa)]4(H2O)}n (2), (L1 = bis(4-(1H-benzo[d]imidazol-1-yl)phenyl)methanone, H2ipa = isophthalic acid, H2pa =... 相似文献
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Crystallography Reports - A cobalt coordination polymer with V-shaped ligands, {[Co0.5(L1) ⋅ (C4H2O4)0.5] ⋅ 0.25H2O}n, (L1 = 4-(1H-imidazol-1-yl)phenyl)methanone, C4H2O4 =... 相似文献
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Crystallography Reports - A cobalt coordination polymer, {[Co(L1)2(H2O)2] · (HCOO)2 · H2O}n, where L1 is a bis(4-(1H-imidazol-1-yl)phenyl)methanone, has been synthesized and characterized... 相似文献
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Crystallography Reports - Zinc coordination polymer with V-shaped ligands, {[Zn(L1) ? (bpda)] ? H2O}n, (1) (L1 = bis(4-(2'-methylimidazol)phenyl)sulfone, H2bpda =... 相似文献
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合成了铜-钠混合金属配位聚合物 [(CuL)2(CH3OO)Na(H2O)4]2 (简写为1)并进行了元素分析和单晶X射线衍射分析,L为{2-(2′-酚基)- Δ 2-噻唑-4-羧酸}.晶体结构分析表明配合物形成Cu4Na2的六核混合金属大环.相邻的Cu4Na2环之间通过进一步的配位作用连结成包含更大的Cu8Na4大环的二维网状结构.该晶体属于三斜晶系Pī空间群,晶胞参数分别为:a = 1.0777(4) nm, b = 1.5221(6) nm, c = 1.6994(6) nm, α = 84.58(1)°, β = 76.31(1)°, γ = 89.97(1) °, V = 2.696 (2) nm3, Z = 2, Mr= 1447.26, dc = 1.783 g·cm-3, T = 293(2) K, μ = 1.816 mm-1, F(000) = 1472, R1 = 0.0794, wR2 = 0.1819 [I>2σ(I)]. 相似文献
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Crystallography Reports - A semi-rigid chiral coordination polymer, {Cd3(4-cpta)2(dpp)2(H2O)}n (1), was synthesized solvothermally with 4-H3cpta (4-H3cpta = 3-(4'-carboxyphenoxy)phthalic acid),... 相似文献
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García-Hernández C. Téllez-López A. Martínez-Otero D. Sánchez-Mendieta V. 《Crystallography Reports》2022,67(7):1175-1182
Crystallography Reports - The three-dimensional cadmium coordination polymer {[Cd4(H2O)2(ita)4(bpe)6]⋅(H2O)26}n (1) (ita = itaconate; bpe = 1,2-bis(4-pyridyl)ethane) was obtained by... 相似文献
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Crystallography Reports - A coordination polymer with the V-shaped ligands, {Cd2(bipmo)2(bdc)2?H2O}n (1), (where bipmo is bis(4-(1H-imidazol-1-yl)phenyl)methanone; H2bdc is... 相似文献
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Semenov V. V. Zolotareva N. V. Novikova O. V. Petrov B. I. Razov E. N. 《Crystallography Reports》2020,65(2):228-232
Crystallography Reports - Poorly soluble protonated erbium bis(1-hydroxyethylidene)diphosphonate tetrahydrate (HEr(H2L)2 · 4H2O), formed as a result of the reaction of erbium carbonate... 相似文献
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Yue Dou Li Guo-Yin Ma Xin-Ru Fu Wen-Ping Zou Ying-Pei Qin Ling Zhang Ming-Dao 《Crystallography Reports》2021,66(7):1262-1267
Crystallography Reports - Two isostructural Co/Ni(II)-based coordination polymers, namely, {[Co1/2(bpba)(H2O)]?2H2O}n (1) and {[Ni1/2(bpba)(H2O)]?2H2O}n (2), where Hbpba = 3,5-bis... 相似文献
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Crystallography Reports - The title compound, 1-(4-(5,6-dihydropyridazin-1(4H)-yl)phenyl)-N-methylmethanesulfonamide (C12H17N3O2S), was isolated as an impurity during the preparation of sumatriptan... 相似文献
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Crystallography Reports - A new six-coordinated Cd(II) polymer {[CdL2(H2O)2]?(H2O)}n (1) (HL = N-nicotinoylglycine) was synthesized with N-nicotinoylglycine, Cd(NO3)2?4H2O, NaOH and... 相似文献
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Brian R. Landry Mark M. Turnbull Brendan Twamley 《Journal of chemical crystallography》2007,37(2):81-86
2,4-Dioxo-4-phenylbutanoic acid, 1, was synthesized as a biproduct of the attempted synthesis of 1,6-bisphenyl-1,3,4,6-hexanetetrone. Crystals of [Cu(H2O)(bipy)
(L)][Cu(bipy)(L)(NO3)] (H2O)(NO3) (L = 2,4-dioxolato-4-phenylbutanoic acid and bipy = 2,2′-bipyridine), 2, were grown by slow evaporation of a solution of Cu(NO3)2·3 H2O, 2,2′-bipyridine, and 1 in a mixture of ethanol and water. The compound crystallized in the triclinic space group P-1 and is made up of two distinct
molecular units each with approximately square pyramidal geometry: a = 10.663(2) ?, b = 13.275(3) ?, c = 15.071(3) ?, α = 80.26(3)°, β = 74.13(3)°, γ = 89.12(3)°. The copper ions are chelated by molecules of 1 and molecules of bipyridine. The molecular units are arrayed in rows held together by pi-stacking interactions and hydrogen
bonding. 相似文献
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Guang Yang 《Journal of chemical crystallography》2004,34(4):269-274
The synthesis of a cobalt(II) complex of tris(1-pyrazolylmethyl)amine (amtp) is reported. The complex [Co(amtp)Cl](BPh4) crystallizes in the space group P-1, with a = 8.979(2), b = 19.329(3), c = 20.251(3) Å, = 93.321(2), = 93.685(3), = 98.930(2)°, and Z = 4. The Co(II) atom is nearly tetrahedrally coordinated by three pyrazole N-atoms and one Cl–. The tertiary amine N-atom of amtp is only weakly coordinated to Co(II) atom at a Co—N(amine) distance of ca 2.40 Å. 相似文献
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Crystallography Reports - A cobalt coordination polymer with the formula of {[Co(L1)(pa)]}n (1) (L1 = bis(4-(1H-benzo[d]imidazol-1-yl)phenyl)methanone, H2pa = phthalic acid) was synthesized under... 相似文献
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