Development of a magnetic measurement device for thin ribbon samples

This paper presents a magnetic measurement device for thin ribbon samples, which are produced by rapid cooling technique. This device enables us to measure magnetic properties easily by only inserting a ribbon sample into a sample holder. The sample holder was made by bakelite to fix any width sample. A long solenoid coil was used to generate a uniform magnetic field and the sample holder was placed at the mid part of the solenoid. The magnetic field strength was measured using a shunt resistor and the magnetic flux density and magnetization in sample ribbons were evaluated by using search coils. The accuracy of measurement was verified with an amorphous metal ribbon sample. Next, we have measured magnetic properties of some magnetic shape memory alloys, which have different compositions. The measured results are compared and we clarified the effect of Sm contents on the magnetic properties.     

A high resolution magnetization sensor for AC loss measurement on cable-in-conduit conductors

A special sensor is proposed for magnetization measurement of superconductors with round cross section under pulsed transversal field. The sensor consists of a saddle shaped pick-up coil attached to the cylindrical superconducting sample, with a controlled geometrical distribution of the turns. The pick up coil carries out a two-dimensional flux integration and the software calculates the loop area in Joules. The sensor has been used during a campaign of ITER subsize conductor tests, showing an excellent agreement (better than 1%) with the results of boil-off calorimetric measurements. The detailed design, the algorithm and the test results are discussed in the paper. Other applications of this test method are proposed.     

A simple electromagnetic method of cyclic loss measurement for superconducting wires in a combined alternating transverse magnetic field and transport current

We measured cyclic losses in a superconducting wire, carrying alternating transport current, simultaneously exposed to an alternating transverse magnetic field. Samples of Bi-2223 Ag-sheathed tapes have configuration of a double-layer non-inductive coil, which itself is a pickup coil to measure the AC losses. Potential taps were attached to both terminals of the sample coil. The external field was applied along the axis of the sample coil. In this procedure, we can estimate an averaged Poynting's vector on a cylindrical surface between the two layers by means of signals from a pair of the potential taps and from pickup coils for the external magnetic field and the transport current. We can also measure a magnetization and an extended transport-current components of AC losses in addition to a total cyclic loss for a combined alternating external field and transport current. Obtained results are compared with numerical predictions of the critical state model taking into account the magnetic field dependence of critical current density.     

Thickness-shear modes and magnetoelastic waves in a longitudinally magnetized ferromagnetic plate

Magnetoelastic (ME) waves and thickness-shear modes in the ferromagnetic plate are studied. Coupled vibrations of magnetization and shear elastic deformations excited simultaneously by a variable magnetic field propagate in two mutually perpendicular directions: parallel and normal to a surface. For parameters characteristic of isotropic ferromagnet with the sample magnetization and Zeeman field parallel to the surface, resonant frequencies of shear modes are computed and their dispersion law is examined. It is shown that the dependence of dimensional resonances frequencies on wave number k_z of ME wave propagating along saturating field direction occurs. The possibility of excitation of ME waves with different k_z explains multimode character of thickness ME resonances.     

Magnetic particle detection by frequency mixing for immunoassay applications

For magnetic immunoassay applications, a novel magnetic reader for quantification of magnetic particle concentrations has been developed. Upon magnetic excitation at two distinct frequencies incident on the sample, the response signal generated at a sum frequency is detected. The low-frequency field component periodically drives the magnetic particles into saturation, which is probed by the high-frequency field. The appearance of frequency mixing lines is highly specific to the nonlinearity of the superparamagnetic particles’ magnetization. The optimization of field coils, differential pickup coil, preamplifier, demodulators and filters are discussed. The output signal is linear for four orders of magnitude in iron concentration.     

Faraday shields within a solenoidal coil to reduce sample heating: Numerical comparison of designs and experimental verification

A comparison of methods to decrease RF power dissipation and related heating in conductive samples using passive conductors surrounding a sample in a solenoid coil is presented. Full-Maxwell finite difference time domain numerical calculations were performed to evaluate the effect of the passive conductors by calculating conservative and magnetically-induced electric field and magnetic field distributions. To validate the simulation method, experimental measurements of temperature increase were conducted using a solenoidal coil (diameter 3 mm), a saline sample (10 mM NaCl) and passive copper shielding wires (50 μm diameter). The temperature increase was 58% lower with the copper wires present for several different input powers to the coil. This was in good agreement with simulation for the same geometry, which indicated 57% lower power dissipated in the sample with conductors present. Simulations indicate that some designs should be capable of reducing temperature increase by more than 85%.     

Vibration analysis and measurement of a gradient coil insert in a 4 T MRI

High speed switching of current in gradient coils within high magnetic field strength Magnetic Resonance Imaging (MRI) scanners may result in high acoustic sound pressure levels in and around these machines. Many studies have already been conducted to characterize the sound field in and around MRIs and various methods have been investigated to attenuate the noise generated. To characterize the vibration properties of the gradient coil, a modified Finite Element (FE) model was developed according to the dimensional design of an available gradient coil insert and the concentration of the copper windings in the coil. The finite element analysis results were verified through experimental modal testing of the same gradient coil in a free-free state (no boundary constraints). Comparisons show that the FE model predicts the vibration properties extremely accurately. Based on the verified FE model, boundary conditions (supports) were added to the model to simulate the operating condition when the gradient coil insert is in place in an MRI machine. Vibration analysis results from the FE model were again verified through experimental vibration testing with the gradient coil insert installed in a 4 T MRI and excited using swept sinusoidal time waveforms. Through a comparison of the vibration signals generated it was found that the vibration resonances, both from the FE model and the experimental vibration testing, shift to higher frequencies after the boundary constraints were applied, as was expected. The predicted vibration response was very close to that measured from the gradient coil insert in operation. The FE modeling procedure that has been developed could easily be used to accurately predict the vibration properties of other gradient coil designs. Furthermore, the vibration analysis results from the FE model could be used in acoustic noise analysis to predict the sound pressure level produced by different types of input current pulse sequences.     

Femtosecond dynamics of Co thin films on Si support

The ultrafast electron and spin dynamics of Co films was investigated using a femto-second pump-probe technique. The samples were magnetically characterized by means of magnetooptical Kerr effect and non-optical magnetometers, i.e. superconductive quantum interference device and alternating gradient field magnetometer. Time evolution of both, Kerr rotation and ellipticity, was measured at different points of the static hysteresis cycle. This allowed separating magnetic and non-magnetic contributions to the signal. The sample magnetization was found to drop within 200 fs, following the pulse cross-correlation trace, while the magnetization recovery time was found to last few picoseconds.     

Magnetic relaxation in spinel Mo-ferrite and Ti substituted Mo-ferrite

A compensation temperature of 138 K was observed in the temperature-dependent magnetization curves of MoFe₂O₄. Relatively slow magnetization relaxation characterized the transitions between different spin states (compensated and uncompensated). Large magnetic after effect was found in time-dependent magnetization curves after heating or cooling from different characteristic temperatures for different spin states. The magnetic relaxation was nearly independent on magnetic field, supporting the presence of spin states and no involvement of domain structure. For the Ti substituted Mo_0.6Ti_0.4Fe₂O₄ sample, there were a compensation at ∼ 100 K and a maximum of magnetization at ∼ 175 K. Similar results of anomalous magnetic relaxation was observed in Ti substituted Mo-ferrite (Mo_0.6Ti_0.4Fe₂O₄). If the Mo_0.6Ti_0.4Fe₂O₄ sample was heated from 100 K to 235 K, the time-dependent magnetization curve could be considered as a combination of two magnetic relaxation processes. However, if the sample was heated from 100 K to 295 K, the time- dependent magnetization curve became complex. Received 30 October 2001 and Received in final form 21 January 2002     

Sample-Induced Resistance Estimation in Magnetic Resonance Experiments: Simulation and Comparison of Two Methods

Signal-to-noise ratio estimation in magnetic resonance experiments requires the knowledge of sample-induced resistance value, where the sample can be protein solutes, cell suspensions, plants, animals, portions of human body or saline solution phantoms. Many authors studied sample–coil interaction using homogeneous infinitely long cylinders, spheres or half-space as approximations of the sample geometry. However, in real magnetic resonance experiments, both sample shape and dimensions can be very different with respect to these models. This paper describes and compares two different methods developed by the authors for sample-induced resistance estimation, both useful for predicting the performance of radio-frequency coils strictly coupled to the sample, where the knowledge of a sample–coil interaction model permits to estimate the different noise contributors. The main goal of our research is testing the proposed algorithms and finding their limitations by comparing their performances for a simple case which uses a sample simplified geometry. The first method, based on the magnetostatic approach, employs vector potential calculation and can be easily implemented for simple coils and sample geometries. The second method uses finite-difference time-domain algorithm and permits to simulate systems with various geometries, without approximations in sample and coil geometries. Comparison with experimental data, performed on three homebuilt surface coils each of them successively tuned at three different frequencies, demonstrated the differences in accuracy of the developed methods.     

Advanced theory of driven birdcage resonator with losses for biomedical magnetic resonance imaging and spectroscopy

A complete time-dependent physics theory of symmetric unperturbed driven hybrid birdcage resonator was developed for general application. In particular, the theory can be applied for radiofrequency (RF) coil engineering, computer simulations of coil-sample interaction, etc. Explicit time dependence is evaluated for different forms of driving voltage. The major steps of the solution development are shown and appropriate explanations are given. Green's functions and spectral density formula were developed for any form of periodic driving voltage. The concept of distributed power losses based on transmission line theory is developed for evaluation of local losses of a coil. Three major types of power losses are estimated as equivalent series resistances in the circuit of the birdcage resonator. Values of generated resistances in legs and end-rings are estimated. An application of the theory is shown for many practical cases. Experimental curve of B₁ field polarization dependence is measured for eight-sections birdcage coil. It was shown that the steady-state driven resonance frequencies do not depend on damping factor unlike the free oscillation (transient) frequencies. An equivalent active resistance is generated due to interaction of RF electromagnetic field with a sample. Resistance of the conductor (enhanced by skin effect), Eddy currents and dielectric losses are the major types of losses which contribute to the values of generated resistances. A biomedical sample for magnetic resonance imaging and spectroscopy is the source of the both Eddy current and dielectric losses of a coil. As demonstrated by the theory, Eddy current loss is the major effect of coil shielding.     

Cross polarization, radio frequency field homogeneity, and circuit balancing in high field solid state NMR probes

Homogeneous radio frequency (RF) fields are important for sensitivity and efficiency of magnetization transfer in solid state NMR experiments. If the fields are inhomogeneous the cross polarization (CP) experiment transfers magnetization in only a thin slice of sample rather than throughout the entire volume. Asymmetric patterns have been observed in plots of the CP signal versus RF field mismatch for an 800 MHz solid-state NMR probe where each channel is resonated in a single-ended mode. A simple model of CP shows these patterns can be reproduced if the RF fields for the two nuclei are centered at different places in the coil. Experimental measurements using B1 field imaging, nutation arrays on extremely short NMR samples, and de-tuning experiments involving disks of copper incrementally moved through the coil support this model of spatially offset RF fields. We have found that resonating the high frequency channel in a double-ended or "balanced" mode can alleviate this field offset problem, and have implemented this in a three-channel solid state NMR probe of our own design.     

HL—1装置新极向场线圈及其对伏秒数特性的改善

本文描述HL-1装置新极场线圈的设计研制、特点、磁场和铁芯磁化曲线。叙述了各种欧姆安匝分布的伏秒数特性、优化选择以及新线圈对提高等离子体参数的明显作用。     

Time-of-flight flow imaging using NMR remote detection

A time-of-flight imaging technique is introduced to visualize fluid flow and dispersion through porous media using NMR. As the fluid flows through a sample, the nuclear spin magnetization is modulated by rf pulses and magnetic field gradients to encode the spatial coordinates of the fluid. When the fluid leaves the sample, its magnetization is recorded by a second rf coil. This scheme not only facilitates a time-dependent imaging of fluid flow, it also allows a separate optimization of encoding and detection subsystems to enhance overall sensitivity. The technique is demonstrated by imaging gas flow through a porous rock.     

Effects of helical anisotropy on nonlinear voltage response in amorphous wires

The nonlinear voltage response in soft magnetic amorphous wires exciting by an alternating current is studied. The frequency spectrum of the voltage in the pick-up coil wound around the wire with a helical anisotropy is found in the framework of a model based on quasi-static Stoner−Wohlfarth magnetization reversal. The effect of a deviation of the anisotropy axis from the azimuthal direction on the field dependences of amplitudes of voltage harmonics is analyzed. It is shown that the field sensitivity of even harmonics increases with the anisotropy axis deviation angle. The current amplitude range to obtain a maximal field sensitivity of the second harmonic is found. The influence of the skin effect on the frequency spectrum of the pick-up coil voltage is discussed. The results obtained may be of importance for the development of sensors of a weak magnetic field.     

Mixed state ultrasonic attenuation in clean niobium near Hc2

Both longitudinal and shear ultrasonic attenuations and magnetization were measured as a function of magnetic field in the mixed state of two niobium single crystal samples with residual resistivity ratios of 68 and 2665 respectively. Particular attention was paid to the behavior of the attenuation at fields near H_c2. The higher purity sample showed marked frequency dependence of normalized attenuation at frequencies from 10 to 110 MHz. The other sample showed qualitatively similar but less pronounced frequency dependence at frequencies ranging from 10 to 435 MHz. Frequency dependence in both samples was in qualitative agreement with the theoretical results of Cerdeira and Houghton[1]. The attenuation changes near H_c2 at the lowest experimental frequencies were compared quantitatively with the frequency independent theoretical results of Houghton and Maki[2]. Agreement in the less pure sample was within a factor of two of the Houghton-Maki results at both 4·2 and 1·4 K. Quantitative comparison to theory for the purer sample must be qualified by the large observed frequency dependence. However, agreement between theory and experiment was excellent at 4·2 K. At 1·4 K in the purer sample, the theoretical predictions differed from experimental results by factors from two to six for various configurations of magnetic field and ultrasonic propagation and polarization directions. Houghton-Maki predictions of the dependence of ultrasonic attenuation on the geometry of magnetic field and ultrasonic propagation and polarization direction were also examined.     

Investigations of magnetic and dielectric properties of cupric oxide nanoparticles

Cupric oxide nanoparticles of ∼8-10 nm width and 40-45 nm length self assembled as large particles ∼1-1.5 μm have been investigated, in the 10-325 K temperature range, using magnetic and dielectric measurements. In magnetic measurements a single broad peak at ∼230 K in a zero field cooled sample has been observed. Coercivity, in magnetization measurements at 10 K, suggests that the nanoparticles are core-shell type particles with an antiferromagnetic core and a ferromagnetic shell. Dielectric measurements, at various frequencies from 3.7 Hz to 949 kHz, exhibit a sharp peak at 284 K followed by weak anomalies around 213 and 230 K.     

Flux pinning by a barrier on the surface of YBaCuO grains studied in dynamic regime

The model of a surface barrier was found to explain well the observed behaviour in quasi-static magnetization experiments on highT_csuperconductors. We study this phenomenon in dynamic conditions in an AC magnetic field with frequencies ranging from 3 Hz up to 115 kHz. The experimental data recorded on a polycrystalline YBaCuO sample are explained by a model supposing the existence of an intergrain critical state and the barrier on the surface of the grains. The most striking feature we found is the decrease of the surface barrier with increasing frequency.     

Simulations of magnetic microstructure in thin film elements used for programmable motion of magnetic particles

The results of two-dimensional micromagnetic modeling of magnetization patterns in Permalloy ellipses under the influence of rotating constant-amplitude magnetic fields are discussed. Ellipses of two different lateral sizes have been studied, 0.5 μm×1.5 μm and 1 μm×3 μm. The amplitude of the rotating magnetic field was varied between simulations with the condition that it must be large enough to saturate or nearly saturate the ellipse with the field applied along the long axis of the ellipse. For the smaller ellipse size it is found that the magnetization pattern forms an S state and the direction of the net magnetization lags behind the direction of the applied field. At a critical angle of the rotating magnetic field the direction of the magnetization switches by a large angle to a new S state. Both the critical angle and the angle interval of the switch depend on field amplitude. For this new state, it is instead the applied field direction that lags behind the magnetization direction. The transient magnetization patterns correspond to multi-domain patterns including two vortices, but this state never exists for the equilibrated magnetization patterns. The behavior of the larger ellipse in rotating field is different. With the field applied along the long-axis of the ellipse, the magnetization of the ellipse is nearly saturated with a vortex close to each apex of the ellipse. As the field is rotated, this magnetization pattern remains and the net-magnetization direction lags behind the direction of the field until for a certain angle of the applied field an equilibrium multi-domain state is created. Comparisons are made with corresponding experimental results obtained by performing in-field magnetic force microscopy on Permalloy ellipses.     

35kV/90MVA高温超导限流器低温系统

35kV/90MVA高温超导限流器的低温系统是一个开放式的液氮制冷系统,包括一个环形不锈钢杜瓦、真空绝热管、压力及温度传感器、低温阀门以及监控系统.高温超导磁体放置在杜瓦中;监控系统检测杜瓦内液氮的液面,并控制往杜瓦内进行补液.杜瓦内蒸发的氮气通过真空绝热管道直接排放到大气中.分别对不同工况下的液氮蒸发量进行了测量.进...