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本文发展了固体废物连续移动床热解实验系统,热解反应器内气、固相表现为相对独立豹柱塞流,据此确定了反应器的设计原则并完成了设计计算.继而以油泥废物为例介绍了该系统的质量和能量平衡计算,系统的质量损失为7.93%~9.15%,略小于国际同等规模装置的误差,通过能量平衡不仅可以确定出油泥热解过程所需净补充热量大小,还可以能源利用回收效率.该实验装置可以视为回转窑、炉排炉等各种垃圾焚烧过程的原型反应器. 相似文献
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BLa Dencs 《Particle & Particle Systems Characterization》1995,12(6):314-317
The average local velocity of the upward of particles motion was determined in a dense fluidized bed by the means of a fibre optical probe. The probe consists of two independent light gates. The particles passing in front of the light gates reflect the light, generating sign sequences that are analysed by computer. From the average time difference of the sign sequences and from the distance of the light gates, the average local velocity can be calculated. The average local velocity of the particles along the height and diameter of the fluidized bed and also as a function of the fluidization air velocity was examined. It was concluded that the average local velocity is closely correlated with the local porosity of the dense fluidized bed and depends mainly on the fluidization air velocity. Using a fibre optical probe, the optimum range of the fluidization air velocity can be determined. 相似文献
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A mathematical model is proposed to show the evolution of temperature, chemical composition and energy release or transfer in slugs, clouds and particulate phase, in a fluidized bed where there are slugs, of a mixture of air and propane, moving up through the particulate phase previously set in the state of incipient fluidization with air. The analysis begins as the slugs are formed at the orifices of the distributor, until they explode inside the bed or emerge at the free surface. The model also makes the analysis of what happens in the gaseous mixture that leaves the free surface of the fluidized bed until the propane is thoroughly burnt. It is essentially built upon a simple quasi-global mechanism for the combustion reaction and the mass and heat transfer equations from the two-phase model of fluidization. The aim was not to propose a new modelling approach, but to combine classical models, one concerning the reaction kinetics and the other the bed hydrodynamic aspects, to obtain a better insight on the events occurring inside a fluidized bed reactor, enhancing the understanding of this type of reactor. Experimental data to balance with the numerical model were obtained through tests on the combustion of commercial propane, in a laboratory scale fluidized bed, using four sand particle sizes: 400–500, 315–400, 250–315 and 200–250 μ m. The mole fractions of CO2, CO and O2 in the flue gases and the temperature of the fluidized bed were measured and compared with the numerical results. 相似文献
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A coaxial induction probe for measuring the charge, size and distance of a passing object is presented. Two different current signals were induced as an object passed the probes. The signals were integrated and Gaussian curves were fitted to the data. According to simulations done with Comsol Multiphysics, the charge, size and distance could be calculated from the amplitudes and widths of the curves. The system was simulated, built and calibrated. It was tested in powder measurements in a fluidized bed device. 相似文献
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Electrostatic charge generation within gas–solid fluidized bed reactors has been a concern to industry for many years. Over the years, numerous methods for measuring this phenomenon within a fluidization column have been proposed. This paper focuses on the design of a new method that minimizes effects such as extra charging due to particle handling and bed hydrodynamic disruption due to the location of the measurement device. In addition, the new method provides the bulk charge of the bed particles rather than a local measurement. The device is flexible and can be adapted to a range of fluidization columns. The new method developed consisted of a Faraday cup placed within the windbox of a fluidization column. The distributor plate was designed in such a way that it can be automatically opened to drop the charged fluidizing particles into the Faraday cup below. The new measurement technique was validated by conducting fluidization experiments in a system consisting of a 0.10 m in diameter carbon steel column with glass beads as the fluidizing particles. The technique was proven to be suitable for measuring the total net electrostatic charges in gas–solid fluidized beds. 相似文献
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Fawzi Salama Andrew Sowinski Khaled Atieh Poupak Mehrani 《Journal of Electrostatics》2013,71(1):21-27
The distribution of charge within the wall fouling region and bulk of a fluidized bed reactor was investigated. Experiments were conducted in a 0.1 m in diameter carbon steel fluidization column under atmospheric conditions. Polyethylene particles were fluidized with extra dry air at 1.5 the minimum fluidization velocity (bubbling flow regime) for 1 h. Using an online Faraday cup measurement technique, the net charge-to-mass ratio (q/m), as well as the size distribution of all particles adhered to the column wall and those in the bulk of the bed was determined. The wall particles were found to be predominantly negatively charged while those which did not adhere to the wall were predominantly positively charged. The charge distribution within each region was then investigated by a custom made charged particle separator that separated the particles according to their charge magnitude and polarity. It was determined that although the net charge of the wall layer particles was negative, a significant amount of positively charged particles existed within each sample and therefore the entire wall particle layer. This suggests that the wall layer was formed through layering between positively and negatively charged particles. Particles in the bulk of the bed also consisted of bipolarly charged particles. 相似文献
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针对气固流化床中风帽故障影响流化质量问题,本文提出一种能够快速精确地检测出风帽故障位置和类型的声发射检测方法;声发射技术是一种实时、在线、非侵入流场的声波检测方法,利用均匀安装在流化床分布板下方的声发射传感器进行定位测量;采集气固流化床内颗粒撞击分布板产生的声信号,对该信号进行多尺度小波包分解,找出特征频段,由各个测点声发射信号总能量对比可以直观反应风帽故障存在位置,而各尺度能量分率的变化能进行故障类型判断;这种实时测量方法能更早,更精确的对风帽破损情况进行准确的判断。 相似文献
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Jinchen Ma Jinxing Wang Xin Tian Haibo Zhao 《Proceedings of the Combustion Institute》2019,37(4):4389-4397
Conventional air incineration of plastic waste has been considered as one of important sources of polychlorinated dibenzo-p-dioxins and dibenzofurans (PCDD/Fs) through de novo synthesis and precursor conversion. Chemical looping combustion (CLC) is an attractive technology for the conversion of plastic wastes to energy with the potential to drastically suppress the formation of PCDD/Fs. In this paper, the iG-CLC (in-situ gasification CLC) experiments of plastic waste were implemented in a semi-continuously operated fluidized bed reactor, which actually simulates the fuel reactor of a continuously-operated interconnected fluidized bed reactor. A kind of low-cost material, natural iron ore without/with 5 wt% CaO adsorbent through the ultrasonic impregnation method, was used as oxygen carrier (OC). Firstly, some key performances of the reactor system, such as the relevance of the bed inventory to the flow rate of fluidizing agent as well as the relationship between the feeding rate and overflow rate of OC, were calibrated. Then, 90 min of single experiment was conducted for each experimental case and an accumulative operation of more than 10 h was attained. Typically, the combustion efficiency can reach at about 98%, and both the carbon conversion and CO2 yield can approach to 95% at 900 °C and input thermal power of 150 W with a mixture of 5 vol% H2O and 95 vol% N2 as the fluidizing agent (UFR/Umf = 3). Moreover, the results obtained in the semi-continuously operated fluidized bed reactor demonstrated that CaO decoration to iron ore is conductive to suppressing the formation of chlorobenzene (as a toxic matter and precursor/intermediate of PCDD/Fs) and does not obviously deteriorate the OC performance. 相似文献
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In this paper we explore the global dynamics of an agent-type model for bubbles in gas-fluidized beds and demonstrate that these features are consistent with experimentally observed behavior. The model accounts for the simultaneous interactions of thousands of individual bubbles and includes mass-transfer and first-order reactions between the gas and solids so that the impact of the dynamics is reflected in reactant conversion. We start with model parameters that have been demonstrated to produce time average behavior consistent with experimental reactor measurements. By observing the temporal variations of spatially averaged bubble properties, we are able to clearly distinguish the onset of global low-dimensional features that appear to be consistent with previous observations. The most prominent of these features is a large-scale oscillation that exhibits intermittency with power-law scaling in the vicinity of a critical gas flow. We show that the oscillation occurs as the result of a globally synchronized horizontal movement of the bubbles toward the center of the reactor. The oscillation appears to be consistent with the occurrence of the so-called "slugging" phenomenon, which is known to have large effects on fluidized bed reactor performance. Although this model can clearly be further improved, its success in replicating several of the key features of slugging indicates that this approach can serve as a useful tool for understanding and possibly controlling fluidized bed dynamics. We also conjecture that this model may be useful for more generally understanding the occurrence of global features in high-dimensional, multi-agent systems. 相似文献
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本文在流化床上对玉米芯进行了快速热解制取生物油的试验研究.首先在非催化条件下考察了温度、气体流量、床高和物料粒径对热解产物产率的影响,得到了制取生物油的最优工况.在此工况下进行了催化热解试验,研究了FCC催化剂对热解产物产率和生物油品质的影响.结果表明,最优工况下生物油产率为56.8%.同未加催化剂相比,FCC催化剂的存在使得生物油中油组分和焦炭的产率降低,不凝结气体、水分和焦的产率增加.分级冷凝系统的应用较好的实现了重油、轻油和水的分离.对催化条件下第二级冷凝器收集的生物油分析表明,其油组分的氧含量和高位热值分别为13.64%和36.7 MJ/kg,具有很好的应用前景. 相似文献
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A novel continuous process is used for production of carbon nanotubes (CNTs) by catalytic chemical vapor deposition (CVD) of methane on iron floating catalyst in situ deposited on MgO in a fluidized bed reactor. In the hot zone of the reactor, sublimed ferrocene vapors were contacted with MgO powder fluidized by methane feed to produce Fe/MgO catalyst in situ. An annular tube was used to enhance the ferrocene and MgO contacting efficiency. Multi-wall as well as single-wall CNTs was grown on the Fe/MgO catalyst while falling down the reactor. The CNTs were continuously collected at the bottom of the reactor, only when MgO powder was used. The annular tube enhanced the contacting efficiency and improved both the quality and quantity of CNTs.The SEM and TEM micrographs of the products reveal that the CNTs are mostly entangled bundles with diameters of about 10-20 nm. Raman spectra show that the CNTs have low amount of amorphous/defected carbon with IG/ID ratios as high as 10.2 for synthesis at 900 °C. The RBM Raman peaks indicate formation of single-walled carbon nanotubes (SWNTs) of 1.0-1.2 nm diameter. 相似文献
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超低浓度煤层气由于甲烷含量低、浓度变化大而较难加以利用。采用实验和数值模拟的方法,研究了超低浓度煤层气在流化床中燃烧特性,得到燃烧产物的轴向分布规律,分析了进气浓度、床层温度、流化风速等因素对甲烷浓度轴向分布的影响。研究结果表明:随着床层高度的增加,无量纲甲烷浓度逐渐减小,在床层表面达到最小值,然后突然增加,随后达到稳定。实验范围内,CO浓度均小于20mL/m~3减小进气浓度、增加床层温度、降低流化风速部会使相同床层高度处的无量纲甲烷浓度减小。燃烧反应主要发生在密相区,随着进气浓度的减小、床层温度的增加、流化风速的降低,反应区域逐渐向床层下部移动。 相似文献
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本文发展一种基于电感耦合等离子体(ICP)技术的烟气镉和锌的在线测量方法,连续测定煤燃烧烟气中镉和锌的瞬时浓度,从而全面跟踪镉和锌的挥发释放过程。实验得到优化的ICP(功率1400W)进气流速为:样品气体,0.03L/min;氩气,0.16 L/min。在线测量系统与流化床实验装置配备在一起,对煤燃烧烟气中镉和锌的浓度进行在线测量。温度对重金属的蒸发有很大影响,温度增加有利于其蒸发,但不是呈线性关系。重金属与飞灰颗粒在高温下反应生成稳定化合物,从而抑制了重金属的挥发。该技术对于研究燃烧过程重金属的释放和控制过程,是一种有用的工具。 相似文献
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We report initial NMR studies of gas dynamics in a particle bed fluidized by laser-polarized xenon (129Xe) gas. We have made preliminary measurements of two important characteristics: gas exchange between the bubble and emulsion phases and the gas velocity distribution in the bed. We used T2* contrast to differentiate the bubble and emulsion phases by choosing solid particles with large magnetic susceptibility. Experimental tests demonstrated that this method was successful in eliminating 129Xe magnetization in the emulsion phase, which enabled us to observe the time dependence of the bubble magnetization. By employing the pulsed field gradient method, we also measured the gas velocity distribution within the bed. These results clearly show the onset of bubbling and can be used to deduce information about gas and particle motion in the fluidized bed. 相似文献