Derivatization and determination of arsenic in marine samples by gas chromatography with electron capture detection |
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Authors: | K. W. M. Siu S. Y. Roberts S. S. Berman |
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Affiliation: | (1) Division of Chemistry, National Research Council of Canada, Montreal Road, K1A OR9 Ottawa, Ontario, Canada |
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Abstract: | Summary Arsenic in marine samples was determined by gas chromatography with electron capture detection after derivatization with 2,3-dimercaptopropanol. Biological tissues and sediments were analyzed after acid decomposition. For sea water, arsenic was preconcentrated by coprecipitation with hydrous iron (III) oxide. The results obtained by this approach compare favourably with the certified values of the reference materials analyzed. Presented at the 15th International Symposium on Chromatography, Nürnberg, October 1984 |
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Keywords: | Gas chromatography Derivatization and determination of arsenic Marine samples Electron capture detector |
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