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An efficient and improved procedure for preparation of triflyl azide and application in catalytic diazotransfer reaction |
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| Authors: | Ri-Bai Yan Fan Yang Yanfen Wu Li-He Zhang Xin-Shan Ye |
| Affiliation: | aThe State Key Laboratory of Natural and Biomimetic Drugs, School of Pharmaceutical Sciences, Peking University, Xue Yuan Rd #38, Beijing 100083, China |
| Abstract: | An efficient and improved procedure for preparation of triflyl azide and application in catalytic diazotransfer reaction are described. The amount of highly toxic reagents NaN3 and Tf2O, is significantly reduced comparing with the previous protocol. |
| Keywords: | Diazotransfer reaction Azide Amine Functional group transformation Synthesis |
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