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Synthesis and properties of water-soluble silica nanoparticles |
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| Authors: | O. B. Gorbatsevich D. N. Kholodkov T. S. Kurkin Yu. N. Malakhova D. R. Strel’tsov A. I. Buzin V. V. Kazakova A. M. Muzafarov |
| Affiliation: | 1.N. S. Enikolopov Institute of Synthetic Polymeric Materials,Russian Academy of Sciences,Moscow,Russian Federation;2.A. N. Nesmeyanov of Organoelement Compounds,Russian Academy of Sciences,Moscow,Russian Federation;3.Moscow Technological University, Institute of Fine Chemical Technologies,Russian Academy of Sciences,Moscow,Russian Federation;4.National Research Centre “Kurchatov Institute”,Moscow,Russian Federation |
| Abstract: | Methods for synthesis and optimum conditions of the formation of stable water-soluble silica nanoparticles are presented. The silica nanoparticles were synthesized by the hydrolytic polycondensation of tetraethoxysilane using two methods: under alkaline conditions (Stöber´s method) or in an acetic acid medium followed by the modification by grafting triethylene oxide moieties on the particle surface. The structure of the modified silica nanoparticles was confirmed by the data of IR and NMR spectroscopy. Polydispersity was evaluated by gel permeation chromatography and dynamic light scattering. The formation and stability of Langmuir monolayers of the silica nanoparticles modified by triethylene oxide moieties were studied. |
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