An efficient and facile synthesis of polydentate ligand: pyridylpyrimidine-2-amine under solvent-free conditions |
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Authors: | Shimin Tao Sheng Xia Liangce Rong Changsheng Cao Shujiang Tu |
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Institution: | 1. Jiangsu Key Laboratory of Green Synthetic Chemistry For Functional Materials, College of Chemistry and Chemical Engineering, Xuzhou Normal University, Xuzhou, Jiangsu, 221116, People’s Republic of China
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Abstract: | An efficient and facile synthesis of polydentate ligand pyridylpyrimidine-2-amine via a one-pot reaction of different aromatic aldehydes, 2-acetylpyridine and guanidine carbonate, in the presence of NaOH under solvent-free conditions, is reported. These compounds have four N-donors and they are classic polydentate ligands of many metal ions. Due to employing a one-pot, multicomponent reaction, this method offers several advantages including easy experimental work-up procedure, and lower cost, short reaction time, and especially high yields of products. This paper therefore develops a practical and convenient process for the synthesis of these ligands. |
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