Preparation of acyl fluorides with hydrogen fluoride-pyridine and 1,3-dicyclohexylcarbodiimide |
| |
| Authors: | Chinpiao Chen Chin-Tzu ChienChu-Hsiang Su |
| |
| Affiliation: | Department of Chemistry, National Dong Hwa University, Hualien 974, Taiwan, ROC |
| |
| Abstract: | This work presents an efficient procedure for preparing acyl fluorides by simply reacting carboxylic acid with hydrogen fluoride-pyridine and 1,3-dicyclohexylcarbodiimide (DCC) in dichloromethane. The acyl fluorides were converted in situ to the corresponding benzyl carboxylic esters by adding benzyl alcohol and triethylamine to the reaction mixture. |
| |
| Keywords: | Acyl fluoride Hydrogen fluoride-pyridine 1,3-Dicyclohexylcarbodiimide |
| 本文献已被 ScienceDirect 等数据库收录！ |
