| O-乙基-O-取代苯基-O-[(2-邻苯二甲酰亚胺基)乙基]硫代磷酸酯的合成及其异构化研究 |
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| 引用本文： | 曾强,黄爱聪.O-乙基-O-取代苯基-O-[(2-邻苯二甲酰亚胺基)乙基]硫代磷酸酯的合成及其异构化研究[J].合成化学,1997(2). |
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| 作者姓名： | 曾强 黄爱聪 |
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| 作者单位： | 南开大学元素有机化学研究所 |
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| 摘 要： | 合成了１１个新的硫羰磷酸酯及其１１个异构化产物硫羟磷酸酯，其结构经１ＨＮＭＲ、元素分析证实。研究了温度、溶剂对异构化反应的影响，并对反应机理进行了讨论。
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| 关 键 词： | 硫羰磷酸酯 硫羟磷酸酯 邻苯二甲酰亚胺 |
Syntheses of a Series of O ethyl O substituted Phenyl O (phthalimide)ethylphosphorothionate and Their Isomeric Reaction |
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| Zeng,Qiang Huang,Ai Cong.Syntheses of a Series of O ethyl O substituted Phenyl O (phthalimide)ethylphosphorothionate and Their Isomeric Reaction[J].Chinese Journal of Synthetic Chemistry,1997(2). |
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| Authors: | Zeng Qiang Huang Ai Cong |
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| Abstract: | Phosphorothionates and 11 isomeric compounds (phosphorothiolates) were synthesized by the reaction of O ethyl O substituted phenyl phosphorochoridothionate with 2 hydroxyethyl phthalimide, using Et 3N as catalyst, these compounds were not reported before. In the paper the relationship between yield and reaction condition (such as temperature, solvents) and the reaction mechanism were discussed. |
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| Keywords: | Phosphorothionate Phthalimide |
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