| 电化学法制备Zn-Ni合金晶须 |
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| 引用本文： | 梁镇海,夏玺华.电化学法制备Zn-Ni合金晶须[J].电化学,2008,14(2):180. |
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| 作者姓名： | 梁镇海 夏玺华 |
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| 作者单位： | 太原理工大学化学化工学院,太原理工大学化学化工学院 山西太原030024,山西太原030024 |
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| 摘 要： | 应用电化学方法制备Zn-Ni合金晶须.样品的成分、形貌用XRD、SEM、EDS等方法表征,结果表明,晶须的物相是Ni5Zn21和Ni3Zn22,直径250 nm,长度2~4μm,长径比8~16.同时用循环伏安法探讨了该过程的电化学行为.为晶须的制备提供了一种新的方法.
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| 关 键 词： | Ni5Zn21 Ni3Zn22 晶须 电化学 |
| 收稿时间： | 2008-05-28 |
Preparation of Zn-Ni Alloy Whisker by Electrochemical Method |
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| LIANG Zhen-hai,XIA Xi-hua.Preparation of Zn-Ni Alloy Whisker by Electrochemical Method[J].Electrochemistry,2008,14(2):180. |
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| Authors: | LIANG Zhen-hai XIA Xi-hua |
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| Institution: | LIANG Zhen-hai,XIA Xi-hua(College of Chemistry , Chemical Engineering,Taiyuan University ofTechnology,Taiyuan 030024,Shanxi,China) |
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| Abstract: | The Zn-Ni alloy whiskers were prepared by electrochemical method and were characterized by XRD、SEM and EDS methods.The results showed that Ni5Zn21 and Ni3Zn22 whiskers were obtained with the length of 2~4 μm and the diameter of 250 nm,thereby the rations of length/diameter fell between 8 and 16.The electrochemical behavior was investigated by cyclic voltammetry method simultaneously.A new method was provided on whisker preparation based on this work. |
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| Keywords: | Ni5Zn21 Ni3Zn22 whisker electrochemistry |
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