Fast, ligand- and solvent-free copper-catalyzed click reactions in a ball mill |
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| Authors: | Thorwirth Rico Stolle Achim Ondruschka Bernd Wild Andreas Schubert Ulrich S |
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| Institution: | Institute for Technical Chemistry and Environmental Chemistry (ITUC), Friedrich-Schiller University Jena, Lessingstr. 12, D-07743 Jena, Germany. |
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| Abstract: | A new, ligand- and solvent-free method for the Huisgen 1,3-dipolar cycloaddition (click reaction) was developed using a planetary ball mill. Besides various alkynes and azides, a propargyl functionalized polymer was converted by mill clicking. Moreover, it was possible to carry out a click polymerization in a ball mill. |
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