| 微波照射下H2O2氧化1,2-环己二醇合成己二酸 |
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| 引用本文： | 周民锋,纪顺俊,黄晓英.微波照射下H2O2氧化1,2-环己二醇合成己二酸[J].合成化学,2004,12(1):9-11. |
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| 作者姓名： | 周民锋 纪顺俊 黄晓英 |
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| 作者单位： | 苏州大学化学化工学院,江苏,苏州,215006;苏州大学化学化工学院,江苏,苏州,215006;苏州大学化学化工学院,江苏,苏州,215006 |
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| 基金项目： | theNationalNaturalScienceFoundationofChina( 2 0 1 72 0 3 9) |
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| 摘 要： | 以钨酸钠为催化剂在微波照射条件下，用30％H2O2使1，2-己二醇氧化开环合成己二酸。考察了照射时间、溶液pH值、不同催化剂及催化剂循环使用等对反应的影响，找出了反应的最佳条件。
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| 关 键 词： | 己二酸 1 2-环己二醇 过氧化氢 微波照射 |
Synthesis of Adipic Acid from 1,2-Cyclohexanediol with H2O2 under Microwave Irradiation |
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| Abstract.Synthesis of Adipic Acid from 1,2-Cyclohexanediol with H2O2 under Microwave Irradiation[J].Chinese Journal of Synthetic Chemistry,2004,12(1):9-11. |
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| Authors: | Abstract |
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| Abstract: | Adipic acid was synthesized from 1,2-cyclohexanediol with 30% H2O2 using Na2WO4·2H2O as a catalyst under microwave irradiation. The amounts of catalyst, the irradiation time and different catalysts were investigated and the optimum experimental conditions were found. |
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| Keywords: | adipic acid 1 2-cyclohexanediol H 2O 2 microwave irradiation |
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