| 纳米银膜的制备及其表面增强拉曼光谱研究 |
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| 引用本文： | 乔世宝,司民真,刘仁明,康颐璞.纳米银膜的制备及其表面增强拉曼光谱研究[J].光散射学报,2009,21(2):129. |
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| 作者姓名： | 乔世宝 司民真 刘仁明 康颐璞 |
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| 作者单位： | 楚雄师范学院光谱应用技术研究所,楚雄,675000 |
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| 摘 要： | 纳米银膜是用硝酸银和聚乙烯醇加入去离子水中作为电解液, 以紫外光激发, 用银棒电解而得到的。扫描电镜被用来具体观测了纳米银的形貌, 发现银膜上的颗粒是紧靠在一起的。我们以结晶紫作为探针分子进行了表面增强拉曼散射效应的的测定, 所用设备为便携式拉曼光谱仪。结果表明光谱的检测限为10-10, 具有很好的增强效果, 这为研究表面增强效应提供了一种新的基底。
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| 关 键 词： | 紫外光诱导 电解法 纳米银膜 SERS |
| 收稿时间： | 2009/1/9 |
The Preparation of Nano-silver Film and the Research on Its SERS Effect |
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| QIAO Shi-bao,SI Min-zhen,LIU Ren-ming,KANG Yi-pu.The Preparation of Nano-silver Film and the Research on Its SERS Effect[J].Chinese Journal of Light Scattering,2009,21(2):129. |
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| Authors: | QIAO Shi-bao SI Min-zhen LIU Ren-ming KANG Yi-pu |
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| Institution: | Department of Physics and Electronic Science;Chuxiong Normal University;Chuxiong 675000;China |
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| Abstract: | The mixture of silver nitrate,polyvinyl alcohol,and deionized water are used as the electrolyte,which is induced by UV-light for five minutes.Two silver poles were served as electrode,and a glass slide is put into the electrolyte.Electrolyze for one hour,place for 24 hours and then take out of the glass slide.The scanning electronic microscopy(SEM) reveals that the particles of Nano-silver on glass slide are compact and uniform.With crystal violet(CV) as a testing molecule,a portable Raman spectrometer with... |
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| Keywords: | SERS |
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