| 环己酮与查尔酮的无溶剂Michael加成反应 |
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| 引用本文： | 荣良策,李小跃,王海营,史达清,屠树江. 环己酮与查尔酮的无溶剂Michael加成反应[J]. 有机化学, 2007, 27(10): 1292-1295 |
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| 作者姓名： | 荣良策 李小跃 王海营 史达清 屠树江 |
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| 作者单位： | 徐州师范大学化学系,徐州,221116 |
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| 基金项目： | 徐州师范大学自然科学基金(No.06XLA09)资助项目 |
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| 摘 要： | 以环己酮和查尔酮为原料, 在 NaOH 存在下无溶剂室温研磨反应, 非常方便地得到Michael加成产物. 该方法具有反应条件温和、操作简单和产率较高等优点, 并通过IR, 1H NMR和元素分析确证产物的结构.
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| 关 键 词： | 环己酮 查尔酮 Michael加成 无溶剂 |
| 收稿时间： | 2006-10-19 |
| 修稿时间： | 2006-10-19 |
Solvent-Free Michael Addition Reaction of Cyclohexanone with Chalcone |
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| RONG Liang-Ce,LI Xiao-Yue,WANG Hai-Ying,SHI Da-Qing,TU Shu-Jiang. Solvent-Free Michael Addition Reaction of Cyclohexanone with Chalcone[J]. Chinese Journal of Organic Chemistry, 2007, 27(10): 1292-1295 |
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| Authors: | RONG Liang-Ce LI Xiao-Yue WANG Hai-Ying SHI Da-Qing TU Shu-Jiang |
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| Affiliation: | Department of Chemistry, Xuzhou Normal University, Xuzhou 221116 |
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| Abstract: | A series of Michael addition products of cyclohexanone to chalcone were obtained in the presence of sodium hydroxide under solvent-free condition. The advantages of this procedure were mild reaction conditions, simple protocol, and high yields. The structures of the products were characterized by IR, 1H NMR spectra and elemental analysis. |
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| Keywords: | cyclohexanone chalcone Michael addition solvent-free |
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