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60keV质子辐照对TiNi记忆合金薄膜马氏体相变的影响
引用本文:王治国,祖小涛,雷雨,莫华强,傅永庆.60keV质子辐照对TiNi记忆合金薄膜马氏体相变的影响[J].强激光与粒子束,2004,16(11):1473-1476.
作者姓名:王治国  祖小涛  雷雨  莫华强  傅永庆
作者单位:1. 电子科技大学 应用物理系,四川 成都 610054;2. Department of Engineering, University of Cambridge, Trumpington Street, CB2, 1PZ, Cambridge, UK
基金项目:国家自然科学基金(10175042)资助课题
摘    要: 利用磁控溅射的方法在氧化后的单晶Si基片上制备了TiNi形状记忆合金薄膜,利用示差扫描量热法和原位X射线衍射研究了薄膜的马氏体相变特征。通过60keV质子注入(辐照)薄膜样品研究了H+离子对合金薄膜马氏体相变特征的影响,结果表明氢离子注入后引起了马氏体相变开始Ms和结束点Mf以及逆马氏体相变开始As和结束温度Af的下降,而对R相变开始Rs和结束温度Rf影响不大。掠入射X射线衍射表明H+离子注入后有氢化物形成。H+离子注入形成的氢化物是引起相变点的变化的主要因素。

关 键 词:TiNi形状记忆合金薄膜  H离子注入  马氏体相变  示差扫描量热仪  X射线衍射
文章编号:1001-4322(2004)11-1473-04
收稿时间:2004/1/4
修稿时间:2004年1月4日

Influence of 60keV proton irradiation on the transformation behavior of a TiNi shape memory alloy thin film
WANG Zhi-guo,ZU Xiao-tao,LEI Yu,MO Hua-qiang,FU Yong-qing.Influence of 60keV proton irradiation on the transformation behavior of a TiNi shape memory alloy thin film[J].High Power Laser and Particle Beams,2004,16(11):1473-1476.
Authors:WANG Zhi-guo  ZU Xiao-tao  LEI Yu  MO Hua-qiang  FU Yong-qing
Institution:1. Department of Applied Physics, University of Electronic Science and Technology of China, Chengdu 610054, China;2. Department of Engineering, University of Cambridge, Trumpington Street, CB2, 1PZ, Cambridge, UK
Abstract:In this work, TiNi shape memory alloy films on oxidized single crystal Si substrate were successfully prepared by co-sputtering of TiNi target with a separated Ti target. The transformation behavior was investigated by differential scanning calorimeter (DSC) and in-situ XRD. 60 keV H~ ions implantation shifted martensite transformation start/finish temperature M_s/M_f and austenite transformation start/finish temperature A_s/A_f to lower temperature, whereas H~ implantation had little effect on the R-phase transformation temperatures R_s and R_f. glance incidence XRD results showed that titanium hydride formed after H~ implantation .The change of transformation temperatures can be attributed to the formation of hydride.
Keywords:TiNi shape memory alloy film  Proton irradiation  Martensitic transformation  Differential scanning calorimeter (DSC)  X-ray diffraction (XRD)  
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