Reaction of hydroxyiminoacetophenone withp-toluenesulfonyl chloride and an X-ray diffraction study of the reaction product |
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| Authors: | A E Fedorov V N Nesterov A M Shestopalov |
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| Institution: | (1) N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 117913 Moscow, Russian Federation;(2) A N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 47 Leninsky prosp, 117813 Moscow, Russian Federation |
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| Abstract: | 2-Benzoyloxy-2-phenylmalononitrile is formed instead of the expected oxime tosylate in the reaction of hydroxyiminoacetophenone
withp-toluenesulfonyl chloride. The structure of the product was confirmed unambiguously by X-ray diffraction analysis.
Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 4, pp. 872–874, April, 1997. |
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| Keywords: | hydroxyiminoacetophenone p-toluenesulfonyl chloride 2-benzoyloxy-2-phenylmalononitrile X-ray diffraction analysis |
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