Synthesis of annelated derivatives of tetrafluoro-10<Emphasis Type="Italic">H</Emphasis>-imidazo[1,2-<Emphasis Type="Italic">b</Emphasis>][1,2]benzooxazin-10-one and 2-pentafluorophenylpyrazine 1,4-dioxide by condensation of alicyclic 2-hydroxyamino oximes with pentafluorophenylglyoxal |
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Authors: | S A Amitina I V El’tsov T V Rybalova Yu V Gatilov I A Grigor’v |
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Institution: | (1) N. N. Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch of the Russian Academy of Sciences, 9 prosp. Akad. Lavrent va, 630090 Novosibirsk, Russian Federation |
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Abstract: | Reactions of alicyclic 2-hydroxyamino oximes with pentafluorophenylglyoxal afford mixtures of annelated derivatives of 2-pentafluorophenylpyrazine 1,4-dioxide and tetrafluoro- 10H-imidazo1,2-b]1,2]benzooxazin-10-one. The structures of the latter were established by X-ray diffraction analysis.Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 8, pp. 1636–1639, August, 2004. |
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Keywords: | tetrafluoro-10H-imidazo[1 2-b][1 2]benzooxazin-10-one 2-hydroxyamino oximes pentafluorophenylpyrazine 1 4-dioxides X-ray diffraction analysis |
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