Optimization of Synthesis of 2,4-Dinitrophenylhydrazones under Carbon Dioxide Pressure |
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Authors: | Eremeev A P |
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Institution: | (1) Pod'emtransmash Open Joint-Stock Company, St. Petersburg, Russia |
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Abstract: | Catalytic synthesis of 2,4-dinitrophenylhydrazones formed in the aqueous reaction mixture of aliphatic and aromatic carbonyl derivatives with 2,4-dinitrophenylhydrazine in the presence of carbonic acid protons under pressure of the CO2-H2O a steam-gas mixture was studied for the example of synthesis of p-quinone-mono-2,4-dinitrophenylhydrazone. |
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