| Enantiomeric Separation of Four Chiral Compounds Using Immobilized Cellulose 3, 5-Dimethylphenylcarbamate as Chiral Stationary Phase |
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| 引用本文： | Yong Fei MING Liang ZHAO Hong Li ZHANG Yan Ping SHI Yong Min LI Li Ren CHEN. Enantiomeric Separation of Four Chiral Compounds Using Immobilized Cellulose 3, 5-Dimethylphenylcarbamate as Chiral Stationary Phase[J]. 中国化学快报, 2006, 17(9): 1213-1216 |
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| 作者姓名： | Yong Fei MING Liang ZHAO Hong Li ZHANG Yan Ping SHI Yong Min LI Li Ren CHEN |
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| 作者单位： | Yong Fei MING1，2，Liang ZHAO1，Hong Li ZHANG1，Yan Ping SHI1，Yong Min LI1，Li Ren CHEN1 1 Key Laboratory for Natural Medicine of Gansu Province，Lanzhou Institute of Chemical Physics，Chinese Academy of Sciences，Lanzhou 730000 2 The Graduate School of Chinese Academy of Sciences，Beijing 100039 |
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| 基金项目： | 国家自然科学基金;甘肃省自然科学基金;中国科学院基金 |
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| 摘 要： | The increasing demands for the production of enantiomerically pure compounds in the field of pharmacology, chemistry, biotechnology, chemical engineering, etc., have made enantioselective separations to become one of the most important analytical tasks. H…
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| 关 键 词： | HPLC 光学分离 手性化合物 手性固定相 纤维素 3 5-二甲基苯基氨基甲酸盐 |
| 收稿时间： | 2006-03-20 |
Enantiomeric Separation of Four Chiral Compounds Using Immobilized Cellulose 3, 5-Dimethylphenylcarbamate as Chiral Stationary Phase |
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| Yong Fei MING,Liang ZHAO,Hong Li ZHANG,Yan Ping SHI,Yong Min LI,Li Ren CHEN. Enantiomeric Separation of Four Chiral Compounds Using Immobilized Cellulose 3, 5-Dimethylphenylcarbamate as Chiral Stationary Phase[J]. Chinese Chemical Letters, 2006, 17(9): 1213-1216 |
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| Authors: | Yong Fei MING Liang ZHAO Hong Li ZHANG Yan Ping SHI Yong Min LI Li Ren CHEN |
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| Abstract: | A new chiral stationary phase of 3, 5-dimethylphenylcarbamates of cellulose, chemically bonded to 3-aminopropylsilica gel at the 6-positions of the glucose units, was prepared. The solvent versatility of the CSP was investigated for the enantioselective separation of four pairs of enantiomers using THF and chloroform as non-standard mobile phase eluent in HPLC. The influence of temperature on the resolution was investigated. |
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| Keywords: | HPLC immobilized enantiomeric separation. |
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