| 2,4-二氯-5-异丙氧基苯胺的合成 |
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| 引用本文： | 潘忠稳,凌冰,叶凯文,于淑琴.2,4-二氯-5-异丙氧基苯胺的合成[J].化学研究与应用,2000,12(4):444-445,457. |
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| 作者姓名： | 潘忠稳 凌冰 叶凯文 于淑琴 |
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| 作者单位： | 安徽省化工研究院农药合成室,安徽,合肥,230041 |
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| 摘 要： | 1 前言 2,4-二氯-5-异丙氧基苯胺是重要的染料、医药和农药中间体,特别是合成1,2,4,5- 四取代苯类含氮杂环除草剂如口恶草酮、2-2,4-二氯-5 -(1-甲基乙氧基)苯基]-4-(2-氟乙基)-1,2,4-三嗪-3,5(2H,4H)-二酮等.该中间体合成未见国内文献报道.专利WO 8600072中报道路线是采用间氨基苯酚经酰化、氯化、水解、醚化制得产品(见方程1).
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| 关 键 词： | 2 4-二氯-5-异丙氧基苯胺 合成 结构 |
| 修稿时间： | 1999-04-07 |
SYNTHESIS OF 2,4-DICHLORO-5-ISOPROPYLOXYANILINE |
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| PAN Zhong-wen,LING Bing,YE Kai-wen,YU Shu-qin.SYNTHESIS OF 2,4-DICHLORO-5-ISOPROPYLOXYANILINE[J].Chemical Research and Application,2000,12(4):444-445,457. |
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| Authors: | PAN Zhong-wen LING Bing YE Kai-wen YU Shu-qin |
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| Abstract: | The preparation method of 2,4 dichloro 5 isopropyloxyaniline was studied.The over all yield as high as 38% is remarkedly better than the those reported in the patent WO 8600072.The product was characterized by IR and elemental analysis. |
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| Keywords: | dichloro 5 isopropyloxyaniline synthesis structure8 |
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