Electrosyntheses of freestanding poly (3-(4-fluorophenyl)thiophene) films in boron trifluoride diethyl etherate |
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| Authors: | Liang Shen Zhenhong Wei Qiang Xiao Shouzhi Pu |
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| Institution: | Jiangxi Key Laboratory of Organic Chemistry, Jiangxi Science and Technology Normal University, Nanchang 330013, PR China |
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| Abstract: | High quality free-standing poly (3-(4-fluorophenyl)thiophene) (PFPT) films with conductivity of 10−1 S/cm were electrosynthesized in boron trifluoride diethyl etherate (BFEE) by direct anodic oxidation of the monomer 3-(4-fluorophenyl)thiophene (FPT) on stainless steel sheet. As-formed flexible and shiny PFPT films can be cut into various shapes by a knife or a pair of scissors. The structure, thermal stability and morphology of PFPT films were studied by FT-infrared, UV-vis, Raman spectroscopy thermogravimetric analysis and scanning electron microscopy, respectively. |
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| Keywords: | Inherently conducting polymers Polythiophene Poly (3-(4-fluorophenyl)thiophene) Electrochemical polymerization Freestanding film |
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