A novel trinuclear nickel(II) complex with a Schiff base derived from m-phenylenediamine and diacetyl monoxime |
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| Authors: | František Březina Zdeněk Smékal Zdeněk Šindelář Richard Pastorek Jerzy Mroziňski |
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| Affiliation: | (1) Department of Inorganic and Physical Chemistry, Palaeký University, K!["rcaron"]("/content/r1737328hkg48442/xlarge345.gif") í!["zcaron"]("/content/r1737328hkg48442/xlarge382.gif") kovského 10, 771 47 Olomouc, Czech Republic;(2) Institute of Chemistry, University of Wroclaw, 50-383 Wroclaw, Poland |
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| Abstract: | Summary A tetradentate Schiff base derived from diacetyl monoxime and m-phenylenediamine (H2mphdao2) reacts in MeOH with NiI2 to form the trinuclear complex Ni3(mphdao2)2I2, which was characterized by elemental and thermal analyses, and i.r. and u.v.-vis. spectroscopies. The magnetic properties have been investigated in the 4.2–300 K range. |
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