Synthesis of 1,2 difluoro-1,2-bis(pentafluorophenyl)dichlorane |
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| Authors: | Joshua A Obaleye Lewis C Sams |
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| Institution: | Department of Chemistry, School of Pure and Applied Sciences, Federal University of Technology, Akure, Ondo State Nigeria;Department of Chemistry, Texas Woman''s University, Denton Texas 76204 U.S.A. |
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| Abstract: | 1,2-Difluoro-1,2-bis(pentafluorophenyl)dichlorane is a new class of organic polyvalent chlorine compound. The closeness of the retention time of this compound and that of chloropentafluoro- benzene made its purification difficult. All attempts to obtain this compound in high yield have failed. 1,2-Difluoro-1,2-bis- (pentafluorophenyl)dichlorane is prepared by fluorination of chloropentafluorobenzene at 128°C with elemental fluorine. It has been characterized by 19F n.m.r., i.r., mass spectroscopy and elemental analysis. |
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| Keywords: | Author to whom correspondence should be addressed |
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