| 壳聚糖接枝聚乙烯吡咯烷酮复合碘膜的制备及其性能 |
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| 引用本文： | 郭瑞,赛明泽,张敏,钟士亮,马文涛,陈蕾,丁德润. 壳聚糖接枝聚乙烯吡咯烷酮复合碘膜的制备及其性能[J]. 应用化学, 2015, 32(5): 0-0. DOI: 10.11944/j.issn.1000-0518.2015.05.140307 |
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| 作者姓名： | 郭瑞 赛明泽 张敏 钟士亮 马文涛 陈蕾 丁德润 |
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| 作者单位： | 上海工程技术大学化学化工学院 上海 201620 |
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| 基金项目： | 国家自然基金资助项目(21305086);国家级大学生创新训练计划项目(201310856012) |
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| 摘 要： | 将CTS接枝PVP后增加了分子间作用力(静电作用)，使聚合物能够更加稳定的吸附碘分子，所以制备的CTS-PVP复合碘膜的抑菌性较CTS-PVP凝胶膜提高显著。
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| 关 键 词： | 壳聚糖 碘 膜 抑菌性能 功能材料 |
| 收稿时间： | 2014-09-03 |
Preparation and Performance of Chitosan Grafted Polyvinyl Pyrrolidone Film with Iodine |
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| GUO Rui,SAI Mingze,ZHANG Min,ZHONG Shiliang,MA Wentao,CHEN Lei,DING Derun. Preparation and Performance of Chitosan Grafted Polyvinyl Pyrrolidone Film with Iodine[J]. Chinese Journal of Applied Chemistry, 2015, 32(5): 0-0. DOI: 10.11944/j.issn.1000-0518.2015.05.140307 |
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| Authors: | GUO Rui SAI Mingze ZHANG Min ZHONG Shiliang MA Wentao CHEN Lei DING Derun |
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| Affiliation: | College of Chemistry and Chemical Engineering, Shanghai University of Engineering Science, Shanghai 201620, China |
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| Abstract: | The CTS-PVP film with iodine was prepared by chitosan(CTS) grafted polyvinyl pyrrolidone(PVP) in the protection of N2 with dimethyl 2, 2'-azobis(2-methylpropionate)(AIBME) as initiator followed by addition of a certain amounts of iodine in ethanol solution and a gelatin solution. The properties of the film were characterized by infrared(IR), scan electron microscopy(SEM), UV-visible spectroscopy(UV-Vis), differential scanning calorimetry(DSC), etc. The UV-Vis spectrum shows a strong absorption between 200~600 nm for the CTS-PVP film with iodine. The glass transition temperature at 319 ℃ indicates a good thermal stability. The antimicrobial test result shows that the inhibition zone diameters increase along with the increasing amounts of CTS-PVP-I2 complex liquid. The inhibition zone diameters against Staphylococcus aureus and Escherichia coli are in the range of 16~36 mm, when the added volume of CTS-PVP-I2 complex fluid is 10 mL or more, implying its high sensitivity and good antibacterial properties. |
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| Keywords: | chitosan iodine film antibacterial properties functional materials |
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