Studies of polycrystalline materials by Pseudo Kossel technique |
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Authors: | E Langer S Däbritz A Röder W Hauffe |
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Institution: | Institut für Oberfl?chenphysik und Mikrostrukturphysik, Technische Universit?t Dresden, D-01062 Dresden, Germany, DE Interdisziplin?res Wissenschaftliches Zentrum für Materialwissenschaften, Martin-Luther-Universit?t Halle, Friedemann-Bach-Platz 6, D-06108 Halle/Saale, Germany, DE
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Abstract: | In contrast to the Kossel Technique the Pseudo Kossel Technique (PKT) is mainly used for investigations of single crystals
to determine the crystal structure, the crystallographic orientation and lattice parameter of the specimens so far. Though
the PKT has yet large possibilities and is well-suited also for micro range investigations, the application for the characterization
of polycrystalline materials is not common. The complicated configuration of the reflex sections in polycrystals, caused by
grain boundary effects, usually makes it very difficult to evaluate them. The studies have been carried out at Al and BaTiO3 polycrystals. Thus, for the first time the successful application of the technique to a ceramic was demonstrated. The dependence
of the reflex length on the grain size was investigated by simulation. It is shown that this technique allows precise determination
of correlation between neighbor grains, since one diffraction pattern contains contributions from several grains. As a result
one obtains for example the relative orientations of neighbor grains, which influence among other things the electrical and
mechanical properties.
Received: 5 November 1998 / Revised: 26 March 1999 / Accepted: 3 April 1999 |
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