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An Efficient Solid-State Synthesis of N-Aryl-2-phenyldiazenecarboxamides
引用本文:Jian Ping LI1*,Qian Fu LUO1,Yi Yang SHEN2,Yu Lu WANG1,Hong WANG1 1College of Chemistry and Environmental Science,Henan Normal University,Xinxiang 453002 2Department of Chemistry,Luoyang Teacher''''s College,Luoyang 471000. An Efficient Solid-State Synthesis of N-Aryl-2-phenyldiazenecarboxamides[J]. 中国化学快报, 2001, 0(2)
作者姓名:Jian Ping LI1*  Qian Fu LUO1  Yi Yang SHEN2  Yu Lu WANG1  Hong WANG1 1College of Chemistry and Environmental Science  Henan Normal University  Xinxiang 453002 2Department of Chemistry  Luoyang Teacher''''s College  Luoyang 471000
作者单位:Jian Ping LI1*,Qian Fu LUO1,Yi Yang SHEN2,Yu Lu WANG1,Hong WANG1 1College of Chemistry and Environmental Science,Henan Normal University,Xinxiang 453002 2Department of Chemistry,Luoyang Teacher's College,Luoyang 471000
基金项目:the financial support from the Natural Science Foundation of Technology Commission of Henan Province.
摘    要:The subject of organic solid-state synthesis is a fascinating one. It has many advantages such as high efficiency and selectivity, easy separation and purification, mild reaction conditions, and environmental acceptability1. In recent years, this method has been widely used in a variety of organic reactions including substitution2, condensation3, oxidation-reduction4, rearrangement5 and elimination6. However, the solid state reaction using K3Fe(CN)6/KOH to oxidize substituted semicarbazides…


An Efficient Solid-State Synthesis of N-Aryl-2-phenyldiazenecarboxamides
Jian Ping LI,Qian Fu LUO,Yi Yang SHEN,Yu Lu WANG,Hong WANG College of Chemistry and Environmental Science,Henan Normal University,Xinxiang. An Efficient Solid-State Synthesis of N-Aryl-2-phenyldiazenecarboxamides[J]. Chinese Chemical Letters, 2001, 0(2)
Authors:Jian Ping LI  Qian Fu LUO  Yi Yang SHEN  Yu Lu WANG  Hong WANG College of Chemistry  Environmental Science  Henan Normal University  Xinxiang
Affiliation:Jian Ping LI1*,Qian Fu LUO1,Yi Yang SHEN2,Yu Lu WANG1,Hong WANG1 1College of Chemistry and Environmental Science,Henan Normal University,Xinxiang 453002 2Department of Chemistry,Luoyang Teacher's College,Luoyang 471000
Abstract:A new and efficient solid-state reaction using K3Fe(CN)6/KOH to oxidize diaryl semicarbazides for preparing azo compounds has been reported. Nine N-aryl-2-phenyl-diazenecarboxamides have been synthesized in excellent yields with simple instrument.
Keywords:Solid-state synthesis   diaryl semicarbazide   N-Aryl-2-phenyldiazenecarboxamide.
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