Three-Component Reaction of 5,5-Dimethylcyclohexan-1,3-dione,Aromatic Aldehydes,and Acetonitrile in the Presence of Chlorosulfonic Acid Forming N-[(2-Hydroxy-4,4-dimethyl-6-oxocyclohexene-1-yl)-aryl-methyl]-acetamides |
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Authors: | Mohammad Anary-Abbasinejad Alireza Hassanabadi Khadijeh Charkhati |
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Affiliation: | 1. Department of Chemistry , Islamic Azad University, Yazd Branch , Yazd, Iran mohammadanary@yahoo.com;3. Department of Chemistry , Islamic Azad University, Yazd Branch , Yazd, Iran |
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Abstract: | A three-component reaction between 5,5-dimethylcyclohexan-1,3-dione (dimedone), aromatic aldehydes, and acetonitrile in the presence of chlorosulfonic acid afforded N-[(2-hydroxy-4,4-dimethyl-6-oxocyclohexene-1-yl)-aryl-methyl]-acetamides in good yields. The temperature-dependent 1H NMR of one of the products has been investigated. |
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Keywords: | Aromatic aldehydes chlorosulfonic acid 5,5-dimethylcyclohexan-1,3-dione multicomponent reaction temperature-dependent 1H NMR |
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