New Effective Synthetic Method for Preparation of N,N-Dichlorocarbamates |
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Authors: | P K Gutch Ravindra Singh S Prabha M V S Suryanarayana |
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Institution: | 1. Synthetic Chemistry Division, Defence Research and Development Establishment , Gwalior , India pkgutch@rediffmail.com;3. Synthetic Chemistry Division, Defence Research and Development Establishment , Gwalior , India;4. School of Studies in Chemistry, Jiwaji University , Gwalior , India |
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Abstract: | A rapid, efficient, economical, and easy-to-scale method for the effective conversion of carbamates to corresponding N,N-dichlorocarbamates by using sodium hypochlorite in acidic medium has been described. N,N-Dichlorocarbamates were obtained in quantitative yield through a simple workup in reduced reaction time. Additional information ACKNOWLEDGMENT We thank Dr. R. Vijayaraghavan, director, Defence Research and Development Establishment, Gwalior, for his keen interest and encouragement. |
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Keywords: | Acidic medium sodium hypochlorite substituted N N-dichlorocarbamates |
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