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A Microwave Promoted New Condensation Reaction of Aryl Ketones With Triethyl Ortho-Formate
Authors:Jianhua Yu  Yulai Hu  Qibin Huang  Ronghua Ma  Shiyan Yang
Affiliation:1. Beijing Institute of Pharmaceutical Chemistry , Box 1044-301, Beijing, 102205, PR China;2. State Key Laboratory for Oxo Synthesis and Selective Oxidation , Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences , Lanzhou, 730000, PR China
Abstract:Under microwave irradiation, boron trifluoride has been found to mediate a new condensation reaction of aryl ketones with triethyl orthoformate to give a series of new products (C1-C10) is described. The compounds were first reported. Their structure were determined by IR, MS, and 1H /13C NMR spectra.
Keywords:
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