A Microwave Promoted New Condensation Reaction of Aryl Ketones With Triethyl Ortho-Formate |
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Authors: | Jianhua Yu Yulai Hu Qibin Huang Ronghua Ma Shiyan Yang |
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Affiliation: | 1. Beijing Institute of Pharmaceutical Chemistry , Box 1044-301, Beijing, 102205, PR China;2. State Key Laboratory for Oxo Synthesis and Selective Oxidation , Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences , Lanzhou, 730000, PR China |
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Abstract: | Under microwave irradiation, boron trifluoride has been found to mediate a new condensation reaction of aryl ketones with triethyl orthoformate to give a series of new products (C1-C10) is described. The compounds were first reported. Their structure were determined by IR, MS, and 1H /13C NMR spectra. |
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