Microwave Assisted One Pot Synthesis of Substituted 3-Formyl Benzoates Using Vilsmeier Reagent |
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Authors: | Srinivasan Selvi Paramasivan T. Perumal |
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Affiliation: | Organic Chemistry Division , Central Leather Research Institute , Adyar, Chennai, 600 020, INDIA Fax: E-mail: ptperumal@hotmail.com |
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Abstract: | A facile one pot conversion of alkyl diacylacetates to 2,6-dichloro-3-formyl benzoates using Vilsmeier reagent in a two pronged strategy - conventional heating and microwave irradiation method is reported. The reaction time has been brought down from hours to seconds in microwave irradiation method. |
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Keywords: | Betulinic acid Chromium oxide Oxidation Solid supported reagent |
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