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One-Pot Synthesis of 2-Amino-5,10-dihydro-5,10-dioxo-4-phenyl-4H-benzo[g]chromene Derivatives Catalyzed by ZnCl2
Authors:V. Srinivas
Affiliation:Department of Chemistry , National Institute of Technology , Warangal , India
Abstract:An efficient one-pot synthesis of 2-amino-5,10-dihydro-5,10-dioxo-4-phenyl-4H-benzo[g]chromene derivatives has been achieved by the reaction of 2-hydroxynaphthalene-1,4-dione, cyanothioacetamide, and aromaticaldehyde in EtOH at room temperature catalyzed by ZnCl2. The structures of the products were characterized by infrared, 1H NMR, mass, and elemental analysis.

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ACKNOWLEDGMENT

We thank the University Grants Commission, New Delhi (F. No. 32-201/2006 (SR)), for financial support.
Keywords:Benzo[g]chromene  cyanothioacetamide  lawsone  one-pot synthesis  ZnCl2
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