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Simple and Efficient Method for the Preparation of Aryl Azides Using Sonication
Authors:Vikas N. Telvekar  Kulbhushan A. Sasane
Affiliation:1. Department of Pharmaceutical Sciences and Technology , Institute of Chemical Technology , Matunga , Mumbai , India vikastelvekar@rediffmail.com;3. Department of Pharmaceutical Sciences and Technology , Institute of Chemical Technology , Matunga , Mumbai , India
Abstract:An efficient procedure for the preparation of aryl azides using sonication is described. The convenient sonication-mediated azidation protocol is applicable to aryl compounds under mild conditions with aqueous solution of sodium dichloroiodate and sodium azide. Aryl azides were obtained in excellent yields from a variety of aryl compounds in short reaction times without affecting sensitive functional groups.
Keywords:Aryl azides  sodium azide  sodium dichloroiodate  sonication
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