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The Synthesis of 1,3-Bis(Phenylseleno)-2-Propanol |
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| Authors: | Yulai Hu Yunsheng Xi Jin-Xian Wang Zhengyin Du Kai Zhao |
| Institution: | 1. Institute of Chemistry, Department of Chemistry , Northwest Normal University , 95 An Ning Road(E), Lanzhou, 730070, P R China;2. Institute of Chemical Industry, Synthetic Rubber Factory, Lanzhou Chemical Industry Corporation , Lanzhou, 730060, P R China |
| Abstract: | A general and efficient synthetic method of 1,3-bis(phenylseleno)-2-propanol by reducing diphenyl diselenides with sodium borohydride in basic environment and then reacting with epichlorohydrin are described. |
| Keywords: | Alcohols Dess–Martin periodinane hypervalent iodine(V) reagents organosulfonic acids α-organosulfonyloxy ketones" target="_blank">α-organosulfonyloxy ketones solvent-free reaction condition |