Synthesis of a Bicyclic Diamine Derived from Kemp's Acid |
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Authors: | Harald Schmaderer Andreas Hohenleutner |
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Institution: | Institute of Organic Chemistry, University of Regensburg , Regensburg, Germany |
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Abstract: | A bicyclic diamine with defined and stable conformation in solution was prepared from Kemp's triacid. The efficient four-step synthesis of the Boc-protected diamine requires only a single purification by column chromatography. X-ray analysis and NMR spectroscopy confirm the structure of the diamine in the solid state and in solution. |
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Keywords: | Diamine Kemp's triacid piperidine |
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