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Synthesis of a Bicyclic Diamine Derived from Kemp's Acid
Authors:Harald Schmaderer  Andreas Hohenleutner
Institution:Institute of Organic Chemistry, University of Regensburg , Regensburg, Germany
Abstract:A bicyclic diamine with defined and stable conformation in solution was prepared from Kemp's triacid. The efficient four-step synthesis of the Boc-protected diamine requires only a single purification by column chromatography. X-ray analysis and NMR spectroscopy confirm the structure of the diamine in the solid state and in solution.
Keywords:Diamine  Kemp's triacid  piperidine
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