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Microwave Heating in Organic Synthesis: Decarboxylation of Malonic Acid Derivatives in Water |
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| Authors: | Cynthia Lynn Zara Thomas Jin Raymond J. Giguere |
| Affiliation: | Department of Chemistry , Skidmore College , Saratoga Springs, NY, 12866–1632, USA |
| Abstract: | Microwave heating permits rapid decarboxylation (15 min, 80–98% isolated yields) of malonic acids in water when employing a microwave autoclave mode and high reaction temperature and power (190°C; 800 Watts). |
| Keywords: | |