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Synthesis of Thia-calix[4]arene Hydroxamic Acids by Microwave Irradiation
Authors:Y K Agrawal  J P Pancholi
Institution:1. Analytical Laboratory, Institute of Pharmacy and Faculty of Science, Nirma University of Science and Technology , Ahmedabad, India drykagrawal@yahoo.com;3. Analytical Laboratory, Institute of Pharmacy and Faculty of Science, Nirma University of Science and Technology , Ahmedabad, India
Abstract:Thia-calix4]arene hydroxamic acids have been synthesized by partial reduction of nitro-thia-calix4]arenes with hydrazine hydrate, Rn/Ni, and their coupling with benzoyl chloride under the influence of microwave irradiation with 90–95% yield and 3–6 min reaction time.
Keywords:Microwave irradiation  thia-calix[4]arene
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