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Efficient One-Pot Synthesis of Tetrahydrobenzo[c]xanthene-1,11-dione Derivatives Under Microwave Irradiation
Authors:Xiao-Jun Sun  Jian-Feng Zhou  San-Jun Zhi
Affiliation:1. School of Chemistry and Chemical Engineering, Huaiyin Normal University , Huaian , China sunxiaojun100@126.com;3. School of Chemistry and Chemical Engineering, Huaiyin Normal University , Huaian , China
Abstract:An efficient one-pot condensation of 4-hydroxylcoumarin, aromatic aldehydes, and 5,5-dimethylcyclohexane-1,3-dione has been achieved with molecular iodine as a catalyst via conventional heating and microwave irradiation techniques, and thus a variety of new tetrahydrobenzo[c]xanthene-1,11-dione derivatives were prepared in good yields.
Keywords:4-Hydroxylcoumarin  microwave irradiation  molecular iodine  one-pot synthesis
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