Crystal structure of bis(isothiocyanato)[2,6-diacetylpyridine bis(4-hydroxybenzoylhydrazone)]Fe(III) Chloride bis(dimethylformamide) solvate期刊界 All Journals 搜尽天下杂志传播学术成果专业期刊搜索期刊信息化学术搜索

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Crystal structure of bis(isothiocyanato)[2,6-diacetylpyridine bis(4-hydroxybenzoylhydrazone)]Fe(III) Chloride bis(dimethylformamide) solvate

Authors:	N Dilek B Güne? O Büyükgüngör R Güp

Institution:	1. Department of Physics, Arts and Sciences Faculty, Aksaray University, 68100, Aksaray, Turkey 2. Department of Physics Education, Gazi Education Faculty, Gazi University, 06500, Teknikokullar, Ankara, Turkey 3. Department of Physics, Arts and Sciences Faculty, Ondokuz Mayis University, 55139, Kurupelit, Samsun, Turkey 4. Department of Chemistry, Arts and Sciences Faculty, Mu?la University, 48000, K?tekli, Mu?la, Turkey

Abstract:	The crystal structure of title compound (Fe(C₂₅H₂₁N₇O₄S₂)] · 4(C₃NOH₇), where C₃NOH₇ is dimethylformamide, DMF) was determined by the X-ray diffraction method. This compound crystallizes in the monoclinic C2/c space group, Z = 4. Unit cell parameters are: a = 13.6080(5), b = 17.6375(7), c = 19.5571(6) Å, β = 108.753(2)°. The N-H...O and O-H...O interactions stabilize the molecules in the lattice. The structure contains also the solvent dimethylformamide molecules, which are connected with intermoleculer hydrogen bond. The O atoms of DMF molecules take place as acceptor atoms.

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