Polyalkoxybenzenes from plant material 6. Synthesis of 3-methyl-3,4-dihydroisoquinolines from apiol |
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| Authors: | Yu. V. Shklyaev A. A. Smolyak S. I. Firgang L. D. Konyushkin |
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| Affiliation: | 1217. Institute of Technical Chemistry, Ural Branch of the Russian Academy of Sciences, 3 ul. Akad. Koroleva, 614013, Perm, Russian Federation
2217. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 119991, Moscow, Russian Federation
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| Abstract: | A number of dihydroisoquinolines were synthesized by the reaction of apiol, a natural allylbenzene, with nitriles. When methyl thiocyanate was used as the nitrile component, the formation of 2-azaspiro[4.5]deca-1,6,9-trien-8-one derivatives, the spiroheterocyclization product, was also observed. |
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