| 新型苯并噻吩七元稠环芳烃衍生物的合成 |
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| 引用本文： | 王静,李斌.新型苯并噻吩七元稠环芳烃衍生物的合成[J].合成化学,2012,20(3):320-323. |
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| 作者姓名： | 王静 李斌 |
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| 作者单位： | 1. 商丘师范学院化学系,河南商丘,476000
2. 兰州大学功能有机分子化学国家重点实验室,甘肃兰州,730000 |
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| 基金项目： | 国家自然科学基金资助项目 |
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| 摘 要： | 以2,3,4,5-四碘代噻吩为起始原料,经Suzuki偶联反应和三氯化铁氧化成环反应,合成了三个新型的苯并噻吩七元稠环芳烃衍生物,其结构经1H NMR,13C NMR,MS,IR和元素分析表征。
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| 关 键 词： | 苯并噻吩 Suzuki偶联反应 稠环芳烃 合成 |
Synthesis of New Seven-ring-fused Benzothiophene Derivatives |
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| WANG Jing
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LI Bin.Synthesis of New Seven-ring-fused Benzothiophene Derivatives[J].Chinese Journal of Synthetic Chemistry,2012,20(3):320-323. |
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| Authors: | WANG Jing LI Bin |
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| Institution: | 1.Department of Chemistry,Shangqiu Normal University,Shangqiu 476000,China; 2.State Key Laboratory of Applied Organic Chemistry,Lanzhou University,Lanzhou 730000,China) |
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| Abstract: | Three new seven-ring-fused benzothiophene derivatives were successfully synthesized from 2,3,4,5-tetraiodothiophene by Suzuki coupling reaction and the oxidative cyclization reaction using ferric chloride as an oxidant.The structures were characterized by 1H NMR,13C NMR,MS,IR and elemental analysis. |
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| Keywords: | benzothiophene Suzuki coupling reaction ring-fused benzothiophene synthesis |
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