| 常温下合成磷酸三苯酯的研究 |
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| 引用本文： | 靳通收,刘利宾,姚剑申,张建设,王爱卿.常温下合成磷酸三苯酯的研究[J].有机化学,2005,25(5):595-597. |
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| 作者姓名： | 靳通收 刘利宾 姚剑申 张建设 王爱卿 |
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| 作者单位： | 河北大学化学与环境科学学院,保定,071002 |
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| 基金项目： | 中国科学院资助项目，高等学校骨干教师资助计划，河北省教育厅科研项目 |
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| 摘 要： | 研究了常温下由苯酚钠悬胶体与三氯氧磷反应合成磷酸三苯酯的工艺条件, 找到了一条比较好的合成方法. 此方法具有操作方便、条件温和、反应时间短、能耗低、腐蚀小、污染少、产物纯、产率高等优点.
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| 关 键 词： | 磷酸三苯酯 苯酚钠悬胶体 常温 合成 |
| 收稿时间： | 2004-8-2 |
| 修稿时间： | 2004-12-4 |
Study on the Synthesis of Triphenyl Phosphate at Room Temperature |
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| JIN Tong-Shou,LIU Li-Bin,YAO Jian-Shen,ZHANG Jian-She,WANG Ai-Qing.Study on the Synthesis of Triphenyl Phosphate at Room Temperature[J].Chinese Journal of Organic Chemistry,2005,25(5):595-597. |
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| Authors: | JIN Tong-Shou LIU Li-Bin YAO Jian-Shen ZHANG Jian-She WANG Ai-Qing |
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| Institution: | (College of Chemistry and Environmental Science, Hebei University, Baoding 071002) |
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| Abstract: | Some technological conditions of the synthesis of triphenyl phosphate by the reaction of sodium phenolate and phosphorus oxychloride were studied, and a better process was found out. This method pro- vided several advantages such as easy operation, mild reaction conditions, short reaction time, low energy consumption, less corrosion, low contamination, high purity and high yield of product. |
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| Keywords: | triphenyl phosphate the suspensoid of sodium phenolate normal temperature synthesis |
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