Ultra-sensitive determination of K, Th, U and other trace impurities in liquid organic scintillators by NAA |
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Authors: | T Goldbrunner R v Hentig G Angloher F v Feilitzsch |
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Institution: | 1. Physik Department der Technischen Universit?t München, James Franck Str., 85748, Garching, Germany
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Abstract: | We present a NAA method to determine ultratraces of K, Th, U and other trace impurities in liquid organic scintillators, which
are known as ultrapure detector materials for neutrino or dark matter experiments. A combined optimization of relevant factors
for sensitive NAA has been realized, leading to a sensitivity for U down to 10−16g/g. Samples of 250 ml have been irradiated up to 120 h at a thermal neutron flux of 5–8·1012·n·cm−2·s−1. Acidic extraction, wet ashing and TBP-extraction are used for radiochemical separations. Finally, coincidence techniques
are applied for increased sensitivity. |
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